Electronic Code of Federal Regulations:

(a) This part identifies hazardous wastes that are restricted from land disposal and defines those limited circumstances under which an otherwise prohibited waste may continue to be land disposed.

(b) Except as specifically provided otherwise in this part or part 261 of this chapter, the requirements of this part apply to persons who generate or transport hazardous waste and owners and operators of hazardous waste treatment, storage, and disposal facilities.

(1) Where persons have been granted an extension to the effective date of a prohibition under subpart C of this part or pursuant to §268.5, with respect to those wastes covered by the extension;

(2) Where persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) Wastes that are hazardous only because they exhibit a hazardous characteristic, and which are otherwise prohibited under this part, or part 148 of this chapter, are not prohibited if the wastes:

(i) Are disposed into a nonhazardous or hazardous injection well as defined under 40 CFR 146.6(a); and

(ii) Do not exhibit any prohibited characteristic of hazardous waste identified in 40 CFR part 261, subpart C at the point of injection.

(4) Wastes that are hazardous only because they exhibit a hazardous characteristic, and which are otherwise prohibited under this part, are not prohibited if the wastes meet any of the following criteria, unless the wastes are subject to a specified method of treatment other than DEACT in §268.40, or are D003 reactive cyanide:

(i) The wastes are managed in a treatment system which subsequently discharges to waters of the U.S. pursuant to a permit issued under section 402 of the Clean Water Act; or

(ii) The wastes are treated for purposes of the pretreatment requirements of section 307 of the Clean Water Act; or

(iii) The wastes are managed in a zero discharge system engaged in Clean Water Act-equivalent treatment as defined in §268.37(a); and

(iv) The wastes no longer exhibit a prohibited characteristic at the point of land disposal (i.e., placement in a surface impoundment).

(d) The requirements of this part shall not affect the availability of a waiver under section 121(d)(4) of the Comprehensive Environmental Response, Compensation, and Liability Act of 1980 (CERCLA).

(e) The following hazardous wastes are not subject to any provision of part 268:

(1) Waste generated by small quantity generators of less than 100 kilograms of non-acute hazardous waste or less than 1 kilogram of acute hazardous waste per month, as defined in §261.5 of this chapter;

(3) Wastes identified or listed as hazardous after November 8, 1984 for which EPA has not promulgated land disposal prohibitions or treatment standards;

(4) De minimis losses of characteristic wastes to wastewaters are not considered to be prohibited wastes and are defined as losses from normal material handling operations (e.g. spills from the unloading or transfer of materials from bins or other containers, leaks from pipes, valves or other devices used to transfer materials); minor leaks of process equipment, storage tanks or containers; leaks from well-maintained pump packings and seals; sample purgings; and relief device discharges; discharges from safety showers and rinsing and cleaning of personal safety equipment; rinsate from empty containers or from containers that are rendered empty by that rinsing; and laboratory wastes not exceeding one per cent of the total flow of wastewater into the facility's headworks on an annual basis, or with a combined annualized average concentration not exceeding one part per million in the headworks of the facility's wastewater treatment or pretreatment facility.

(f) Universal waste handlers and universal waste transporters (as defined in 40 CFR 260.10) are exempt from 40 CFR 268.7 and 268.50 for the hazardous wastes listed below. These handlers are subject to regulation under 40 CFR part 273.

[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 53 FR 27165, July 19, 1988; 53 FR 31212, Aug. 17, 1988; 54 FR 36970, Sept. 6, 1989; 55 FR 22686, June 1, 1990; 58 FR 29884, May 24, 1993; 59 FR 48043, Sept. 19, 1994; 60 FR 25542, May 11, 1995; 61 FR 15663, Apr. 8, 1996; 61 FR 33682, June 28, 1996; 62 FR 26019, May 12, 1997; 64 FR 36488, July 6, 1999; 70 FR 45520, Aug. 5, 2005]

(a) Halogenated organic compounds or HOCs means those compounds having a carbon-halogen bond which are listed under appendix III to this part.

(b) Hazardous constituent or constituents means those constituents listed in appendix VIII to part 261 of this chapter.

(c) Land disposal means placement in or on the land, except in a corrective action management unit or staging pile, and includes, but is not limited to, placement in a landfill, surface impoundment, waste pile, injection well, land treatment facility, salt dome formation, salt bed formation, underground mine or cave, or placement in a concrete vault, or bunker intended for disposal purposes.

(d) Nonwastewaters are wastes that do not meet the criteria for wastewaters in paragraph (f) of this section.

(e) Polychlorinated biphenyls or PCBs are halogenated organic compounds defined in accordance with 40 CFR 761.3.

(f) Wastewaters are wastes that contain less than 1% by weight total organic carbon (TOC) and less than 1% by weight total suspended solids (TSS).

(g) Debris means solid material exceeding a 60 mm particle size that is intended for disposal and that is: A manufactured object; or plant or animal matter; or natural geologic material. However, the following materials are not debris: any material for which a specific treatment standard is provided in Subpart D, Part 268, namely lead acid batteries, cadmium batteries, and radioactive lead solids; process residuals such as smelter slag and residues from the treatment of waste, wastewater, sludges, or air emission residues; and intact containers of hazardous waste that are not ruptured and that retain at least 75% of their original volume. A mixture of debris that has not been treated to the standards provided by §268.45 and other material is subject to regulation as debris if the mixture is comprised primarily of debris, by volume, based on visual inspection.

(h) Hazardous debris means debris that contains a hazardous waste listed in subpart D of part 261 of this chapter, or that exhibits a characteristic of hazardous waste identified in subpart C of part 261 of this chapter. Any deliberate mixing of prohibited hazardous waste with debris that changes its treatment classification (i.e., from waste to hazardous debris) is not allowed under the dilution prohibition in §268.3.

(i) Underlying hazardous constituent means any constituent listed in §268.48, Table UTS—Universal Treatment Standards, except fluoride, selenium, sulfides, vanadium, and zinc, which can reasonably be expected to be present at the point of generation of the hazardous waste at a concentration above the constituent-specific UTS treatment standards.

(j) Inorganic metal-bearing waste is one for which EPA has established treatment standards for metal hazardous constituents, and which does not otherwise contain significant organic or cyanide content as described in §268.3(c)(1), and is specifically listed in appendix XI of this part.

(k) Soil means unconsolidated earth material composing the superficial geologic strata (material overlying bedrock), consisting of clay, silt, sand, or gravel size particles as classified by the U.S. Natural Resources Conservation Service, or a mixture of such materials with liquids, sludges or solids which is inseparable by simple mechanical removal processes and is made up primarily of soil by volume based on visual inspection. Any deliberate mixing of prohibited hazardous waste with soil that changes its treatment classification (i.e., from waste to contaminated soil) is not allowed under the dilution prohibition in §268.3.

[55 FR 22686, June 1, 1990, as amended at 56 FR 3877, Jan. 31, 1991; 57 FR 37270, Aug. 18, 1992; 58 FR 8685, Feb. 16, 1993; 58 FR 29884, May 24, 1993; 59 FR 48043, Sept. 19, 1994; 60 FR 244, Jan. 3, 1995; 61 FR 15597, 15662, Apr. 8, 1996; 61 FR 33682, June 28, 1996; 63 FR 28639, May 26, 1998; 63 FR 65940, Nov. 30, 1998; 64 FR 25414, May 11, 1999; 71 FR 40278, July 14, 2006]

(a) Except as provided in paragraph (b) of this section, no generator, transporter, handler, or owner or operator of a treatment, storage, or disposal facility shall in any way dilute a restricted waste or the residual from treatment of a restricted waste as a substitute for adequate treatment to achieve compliance with subpart D of this part, to circumvent the effective date of a prohibition in subpart C of this part, to otherwise avoid a prohibition in subpart C of this part, or to circumvent a land disposal prohibition imposed by RCRA section 3004.

(b) Dilution of wastes that are hazardous only because they exhibit a characteristic in treatment systems which include land- based units which treat wastes subsequently discharged to a water of the United States pursuant to a permit issued under section 402 of the Clean Water Act (CWA), or which treat wastes in a CWA-equivalent treatment system, or which treat wastes for the purposes of pretreatment requirements under section 307 of the CWA is not impermissible dilution for purposes of this section unless a method other than DEACT has been specified in §268.40 as the treatment standard, or unless the waste is a D003 reactive cyanide wastewater or nonwastewater.

(c) Combustion of the hazardous waste codes listed in Appendix XI of this part is prohibited, unless the waste, at the point of generation, or after any bona fide treatment such as cyanide destruction prior to combustion, can be demonstrated to comply with one or more of the following criteria (unless otherwise specifically prohibited from combustion):

(1) The waste contains hazardous organic constituents or cyanide at levels exceeding the constituent-specific treatment standard found in §268.48;

(2) The waste consists of organic, debris-like materials (e.g., wood, paper, plastic, or cloth) contaminated with an inorganic metal-bearing hazardous waste;

(3) The waste, at point of generation, has reasonable heating value such as greater than or equal to 5000 BTU per pound;

(4) The waste is co-generated with wastes for which combustion is a required method of treatment;

(5) The waste is subject to Federal and/or State requirements necessitating reduction of organics (including biological agents); or

(d) It is a form of impermissible dilution, and therefore prohibited, to add iron filings or other metallic forms of iron to lead-containing hazardous wastes in order to achieve any land disposal restriction treatment standard for lead. Lead-containing wastes include D008 wastes (wastes exhibiting a characteristic due to the presence of lead), all characteristic wastes containing lead as an underlying hazardous constituent, listed wastes containing lead as a regulated constituent, and hazardous media containing any of the aforementioned lead-containing wastes.

[61 FR 15663, Apr. 8, 1996, as amended at 61 FR 33682, June 28, 1996; 63 FR 28639, May 26, 1998]

(a) Wastes which are otherwise prohibited from land disposal under this part may be treated in a surface impoundment or series of impoundments provided that:

(i) Sampling and testing. For wastes with treatment standards in subpart D of this part and/or prohibition levels in subpart C of this part or RCRA section 3004(d), the residues from treatment are analyzed, as specified in §268.7 or §268.32, to determine if they meet the applicable treatment standards or where no treatment standards have been established for the waste, the applicable prohibition levels. The sampling method, specified in the waste analysis plan under §264.13 or §265.13, must be designed such that representative samples of the sludge and the supernatant are tested separately rather than mixed to form homogeneous samples.

(ii) Removal . The following treatment residues (including any liquid waste) must be removed at least annually; residues which do not meet the treatment standards promulgated under subpart D of this part; residues which do not meet the prohibition levels established under subpart C of this part or imposed by statute (where no treatment standards have been established); residues which are from the treatment of wastes prohibited from land disposal under subpart C of this part (where no treatment standards have been established and no prohibition levels apply); or residues from managing listed wastes which are not delisted under §260.22 of this chapter. If the volume of liquid flowing through the impoundment or series of impoundments annually is greater than the volume of the impoundment or impoundments, this flow-through constitutes removal of the supernatant for the purpose of this requirement.

(iii) Subsequent management . Treatment residues may not be placed in any other surface impoundment for subsequent management.

(iv) Recordkeeping. Sampling and testing and recordkeeping provisions of §§264.13 and 265.13 of this chapter apply.

(3) The impoundment meets the design requirements of §264.221(c) or §265.221(a) of this chapter, regardless that the unit may not be new, expanded, or a replacement, and be in compliance with applicable ground water monitoring requirements of subpart F of part 264 or part 265 of this chapter unless:

(i) Exempted pursuant to §264.221 (d) or (e) of this chapter, or to §265.221 (c) or (d) of this chapter; or,

(ii) Upon application by the owner or operator, the Administrator, after notice and an opportunity to comment, has granted a waiver of the requirements on the basis that the surface impoundment:

(A) Has at least one liner, for which there is no evidence that such liner is leaking;

(B) Is located more than one-quarter mile from an underground source of drinking water; and

(iii) Upon application by the owner or operator, the Administrator, after notice and an opportunity to comment, has granted a modification to the requirements on the basis of a demonstration that the surface impoundment is located, designed, and operated so as to assure that there will be no migration of any hazardous constituent into ground water or surface water at any future time.

(4) The owner or operator submits to the Regional Administrator a written certification that the requirements of §268.4(a)(3) have been met. The following certification is required:

I certify under penalty of law that the requirements of 40 CFR 268.4(a)(3) have been met for all surface impoundments being used to treat restricted wastes. I believe that the submitted information is true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment.

(b) Evaporation of hazardous constituents as the principal means of treatment is not considered to be treatment for purposes of an exemption under this section.

[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 52 FR 25788, July 8, 1987; 53 FR 31212, Aug. 17, 1988; 62 FR 26019, May 12, 1997; 63 FR 28639, May 26, 1998; 71 FR 40278, July 14, 2006]

(a) Any person who generates, treats, stores, or disposes of a hazardous waste may submit an application to the Administrator for an extension to the effective date of any applicable restriction established under subpart C of this part. The applicant must demonstrate the following:

(1) He has made a good-faith effort to locate and contract with treatment, recovery, or disposal facilities nationwide to manage his waste in accordance with the effective date of the applicable restriction established under subpart C of this part;

(2) He has entered into a binding contractual commitment to construct or otherwise provide alternative treatment, recovery (e.g., recycling), or disposal capacity that meets the treatment standards specified in subpart D or, where treatment standards have not been specified, such treatment, recovery, or disposal capacity is protective of human health and the environment.

(3) Due to circumstances beyond the applicant's control, such alternative capacity cannot reasonably be made available by the applicable effective date. This demonstration may include a showing that the technical and practical difficulties associated with providing the alternative capacity will result in the capacity not being available by the applicable effective date;

(4) The capacity being constructed or otherwise provided by the applicant will be sufficient to manage the entire quantity of waste that is the subject of the application;

(5) He provides a detailed schedule for obtaining required operating and construction permits or an outline of how and when alternative capacity will be available;

(6) He has arranged for adequate capacity to manage his waste during an extension and has documented in the application the location of all sites at which the waste will be managed; and

(7) Any waste managed in a surface impoundment or landfill during the extension period will meet the requirements of paragraph (h)(2) of this section.

(b) An authorized representative signing an application described under paragraph (a) of this section shall make the following certification:

I certify under penalty of law that I have personally examined and am familiar with the information submitted in this document and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the information is true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment.

(c) After receiving an application for an extension, the Administrator may request any additional information which he deems as necessary to evaluate the application.

(d) An extension will apply only to the waste generated at the individual facility covered by the application and will not apply to restricted waste from any other facility.

(e) On the basis of the information referred to in paragraph (a) of this section, after notice and opportunity for comment, and after consultation with appropriate State agencies in all affected States, the Administrator may grant an extension of up to 1 year from the effective date. The Administrator may renew this extension for up to 1 additional year upon the request of the applicant if the demonstration required in paragraph (a) of this section can still be made. In no event will an extension extend beyond 24 months from the applicable effective date specified in subpart C of part 268. The length of any extension authorized will be determined by the Administrator based on the time required to construct or obtain the type of capacity needed by the applicant as described in the completion schedule discussed in paragraph (a)(5) of this section. The Administrator will give public notice of the intent to approve or deny a petition and provide an opportunity for public comment. The final decision on a petition will be published in theFederal Register.

(f) Any person granted an extension under this section must immediately notify the Administrator as soon as he has knowledge of any change in the conditions certified to in the application.

(g) Any person granted an extension under this section shall submit written progress reports at intervals designated by the Administrator. Such reports must describe the overall progress made toward constructing or otherwise providing alternative treatment, recovery or disposal capacity; must identify any event which may cause or has caused a delay in the development of the capacity; and must summarize the steps taken to mitigate the delay. The Administrator can revoke the extension at any time if the applicant does not demonstrate a good-faith effort to meet the schedule for completion, if the Agency denies or revokes any required permit, if conditions certified in the application change, or for any violation of this chapter.

(h) Whenever the Administrator establishes an extension to an effective date under this section, during the period for which such extension is in effect:

(2) Such hazardous waste may be disposed in a landfill or surface impoundment only if such unit is in compliance with the technical requirements of the following provisions regardless of whether such unit is existing, new, or a replacement or lateral expansion.

(i) The landfill, if in interim status, is in compliance with the requirements of subpart F of part 265 and §265.301 (a), (c), and (d) of this chapter; or,

(ii) The landfill, if permitted, is in compliance with the requirements of subpart F of part 264 and §264.301 (c), (d) and (e) of this chapter; or

(iii) The surface impoundment, if in interim status, is in compliance with the requirements of subpart F of part 265, §265.221 (a), (c), and (d) of this chapter, and RCRA section 3005(j)(1); or

(iv) The surface impoundment, if permitted, is in compliance with the requirements of subpart F of part 264 and §264.221 (c), (d) and (e) of this chapter; or

(v) The surface impoundment, if newly subject to RCRA section 3005(j)(1) due to the promulgation of additional listings or characteristics for the identification of hazardous waste, is in compliance with the requirements of subpart F of part 265 of this chapter within 12 months after the promulgation of additional listings or characteristics of hazardous waste, and with the requirements of §265.221 (a), (c) and (d) of this chapter within 48 months after the promulgation of additional listings or characteristics of hazardous waste. If a national capacity variance is granted, during the period the variance is in effect, the surface impoundment, if newly subject to RCRA section 3005(j)(1) due to the promulgation of additional listings or characteristics of hazardous waste, is in compliance with the requirements of subpart F of part 265 of this chapter within 12 months after the promulgation of additional listings or characteristics of hazardous waste, and with the requirements of §265.221 (a), (c) and (d) of this chapter within 48 months after the promulgation of additional listings or characteristics of hazardous waste; or

(vi) The landfill, if disposing of containerized liquid hazardous wastes containing PCBs at concentrations greater than or equal to 50 ppm but less than 500 ppm, is also in compliance with the requirements of 40 CFR 761.75 and parts 264 and 265.

(i) Pending a decision on the application the applicant is required to comply with all restrictions on land disposal under this part once the effective date for the waste has been reached.

[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 52 FR 25788, July 8, 1987; 54 FR 36971, Sept. 6, 1989; 55 FR 23935, June 13, 1990; 57 FR 37270, Aug. 18, 1992]

(a) Any person seeking an exemption from a prohibition under subpart C of this part for the disposal of a restricted hazardous waste in a particular unit or units must submit a petition to the Administrator demonstrating, to a reasonable degree of certainty, that there will be no migration of hazardous constituents from the disposal unit or injection zone for as long as the wastes remain hazardous. The demonstration must include the following components:

(1) An identification of the specific waste and the specific unit for which the demonstration will be made;

(2) A waste analysis to describe fully the chemical and physical characteristics of the subject waste;

(3) A comprehensive characterization of the disposal unit site including an analysis of background air, soil, and water quality.

(5) Sufficient information to assure the Administrator that the owner or operator of a land disposal unit receiving restricted waste(s) will comply with other applicable Federal, State, and local laws.

(b) The demonstration referred to in paragraph (a) of this section must meet the following criteria:

(1) All waste and environmental sampling, test, and analysis data must be accurate and reproducible to the extent that state-of-the-art techniques allow;

(2) All sampling, testing, and estimation techniques for chemical and physical properties of the waste and all environmental parameters must have been approved by the Administrator;

(3) Simulation models must be calibrated for the specific waste and site conditions, and verified for accuracy by comparison with actual measurements;

(4) A quality assurance and quality control plan that addresses all aspects of the demonstration must be approved by the Administrator; and,

(5) An analysis must be performed to identify and quantify any aspects of the demonstration that contribute significantly to uncertainty. This analysis must include an evaluation of the consequences of predictable future events, including, but not limited to, earthquakes, floods, severe storm events, droughts, or other natural phenomena.

(1) A monitoring plan that describes the monitoring program installed at and/or around the unit to verify continued compliance with the conditions of the variance. This monitoring plan must provide information on the monitoring of the unit and/or the environment around the unit. The following specific information must be included in the plan:

(i) The media monitored in the cases where monitoring of the environment around the unit is required;

(ii) The type of monitoring conducted at the unit, in the cases where monitoring of the unit is required;

(2) Where applicable, the monitoring program described in paragraph (c)(1) of this section must be in place for a period of time specified by the Administrator, as part of his approval of the petition, prior to receipt of prohibited waste at the unit.

(3) The monitoring data collected according to the monitoring plan specified under paragraph (c)(1) of this section must be sent to the Administrator according to a format and schedule specified and approved in the monitoring plan, and

(4) A copy of the monitoring data collected under the monitoring plan specified under paragraph (c)(1) of this section must be kept on-site at the facility in the operating record.

(5) The monitoring program specified under paragraph (c)(1) of this section meets the following criteria:

(i) All sampling, testing, and analytical data must be approved by the Administrator and must provide data that is accurate and reproducible.

(ii) All estimation and monitoring techniques must be approved by the Administrator.

(iii) A quality assurance and quality control plan addressing all aspects of the monitoring program must be provided to and approved by the Administrator.

(e) After a petition has been approved, the owner or operator must report any changes in conditions at the unit and/or the environment around the unit that significantly depart from the conditions described in the variance and affect the potential for migration of hazardous constituents from the units as follows:

(1) If the owner or operator plans to make changes to the unit design, construction, or operation, such a change must be proposed, in writing, and the owner or operator must submit a demonstration to the Administrator at least 30 days prior to making the change. The Administrator will determine whether the proposed change invalidates the terms of the petition and will determine the appropriate response. Any change must be approved by the Administrator prior to being made.

(2) If the owner or operator discovers that a condition at the site which was modeled or predicted in the petition does not occur as predicted, this change must be reported, in writing, to the Administrator within 10 days of discovering the change. The Administrator will determine whether the reported change from the terms of the petition requires further action, which may include termination of waste acceptance and revocation of the petition, petition modifications, or other responses.

(f) If the owner or operator determines that there is migration of hazardous constituent(s) from the unit, the owner or operator must:

(2) Notify the Administrator, in writing, within 10 days of the determination that a release has occurred.

(3) Following receipt of the notification the Administrator will determine, within 60 days of receiving notification, whether the owner or operator can continue to receive prohibited waste in the unit and whether the variance is to be revoked. The Administrator shall also determine whether further examination of any migration is warranted under applicable provisions of part 264 or part 265.

(g) Each petition must include the following statement signed by the petitioner or an authorized representative:

I certify under penalty of law that I have personally examined and am familiar with the information submitted in this petition and all attached documents, and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that submitted information is true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment.

(h) After receiving a petition, the Administrator may request any additional information that reasonably may be required to evaluate the demonstration.

(i) If approved, the petition will apply to land disposal of the specific restricted waste at the individual disposal unit described in the demonstration and will not apply to any other restricted waste at that disposal unit, or to that specific restricted waste at any other disposal unit.

(j) The Administrator will give public notice in theFederal Registerof the intent to approve or deny a petition and provide an opportunity for public comment. The final decision on a petition will be published in theFederal Register.

(k) The term of a petition granted under this section shall be no longer than the term of the RCRA permit if the disposal unit is operating under a RCRA permit, or up to a maximum of 10 years from the date of approval provided under paragraph (g) of this section if the unit is operating under interim status. In either case, the term of the granted petition shall expire upon the termination or denial of a RCRA permit, or upon the termination of interim status or when the volume limit of waste to be land disposed during the term of petition is reached.

(l) Prior to the Administrator's decision, the applicant is required to comply with all restrictions on land disposal under this part once the effective date for the waste has been reached.

(m) The petition granted by the Administrator does not relieve the petitioner of his responsibilities in the management of hazardous waste under 40 CFR part 260 through part 271.

(n) Liquid hazardous wastes containing polychlorinated biphenyls at concentrations greater than or equal to 500 ppm are not eligible for an exemption under this section.

[51 FR 40638, Nov. 7, 1986; 52 FR 21016, June 4, 1987, as amended at 52 FR 25789, July 8, 1987; 53 FR 31212, Aug. 17, 1988; 54 FR 36971, Sept. 6, 1989; 71 FR 40278, July 14, 2006]

(a) Requirements for generators: (1) A generator of hazardous waste must determine if the waste has to be treated before it can be land disposed. This is done by determining if the hazardous waste meets the treatment standards in §268.40, 268.45, or §268.49. This determination can be made concurrently with the hazardous waste determination required in §262.11 of this chapter, in either of two ways: testing the waste or using knowledge of the waste. If the generator tests the waste, testing would normally determine the total concentration of hazardous constituents, or the concentration of hazardous constituents in an extract of the waste obtained using test method 1311 in “Test Methods of Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846, (incorporated by reference, see §260.11 of this chapter), depending on whether the treatment standard for the waste is expressed as a total concentration or concentration of hazardous constituent in the waste's extract. (Alternatively, the generator must send the waste to a RCRA-permitted hazardous waste treatment facility, where the waste treatment facility must comply with the requirements of §264.13 of this chapter and paragraph (b) of this section.) In addition, some hazardous wastes must be treated by particular treatment methods before they can be land disposed and some soils are contaminated by such hazardous wastes. These treatment standards are also found in §268.40, and are described in detail in §268.42, Table 1. These wastes, and soils contaminated with such wastes, do not need to be tested (however, if they are in a waste mixture, other wastes with concentration level treatment standards would have to be tested). If a generator determines they are managing a waste or soil contaminated with a waste, that displays a hazardous characteristic of ignitability, corrosivity, reactivity, or toxicity, they must comply with the special requirements of §268.9 of this part in addition to any applicable requirements in this section.

(2) If the waste or contaminated soil does not meet the treatment standards, or if the generator chooses not to make the determination of whether his waste must be treated, with the initial shipment of waste to each treatment or storage facility, the generator must send a one-time written notice to each treatment or storage facility receiving the waste, and place a copy in the file. The notice must include the information in column “268.7(a)(2)” of the Generator Paperwork Requirements Table in paragraph (a)(4) of this section. (Alternatively, if the generator chooses not to make the determination of whether the waste must be treated, the notification must include the EPA Hazardous Waste Numbers and Manifest Number of the first shipment and must state “This hazardous waste may or may not be subject to the LDR treatment standards. The treatment facility must make the determination.”) No further notification is necessary until such time that the waste or facility change, in which case a new notification must be sent and a copy placed in the generator's file.

(3) If the waste or contaminated soil meets the treatment standard at the original point of generation:

(i) With the initial shipment of waste to each treatment, storage, or disposal facility, the generator must send a one-time written notice to each treatment, storage, or disposal facility receiving the waste, and place a copy in the file. The notice must include the information indicated in column “268.7(a)(3)” of the Generator Paperwork Requirements Table in §268.7(a)(4) and the following certification statement, signed by an authorized representative:

I certify under penalty of law that I personally have examined and am familiar with the waste through analysis and testing or through knowledge of the waste to support this certification that the waste complies with the treatment standards specified in 40 CFR part 268 subpart D. I believe that the information I submitted is true, accurate, and complete. I am aware that there are significant penalties for submitting a false certification, including the possibility of a fine and imprisonment.

(ii) For contaminated soil, with the initial shipment of wastes to each treatment, storage, or disposal facility, the generator must send a one-time written notice to each facility receiving the waste and place a copy in the file. The notice must include the information in column “268.7(a)(3)” of the Generator Paperwork Requirements Table in §268.7(a)(4).

(iii) If the waste changes, the generator must send a new notice and certification to the receiving facility, and place a copy in their files. Generators of hazardous debris excluded from the definition of hazardous waste under §261.3(f) of this chapter are not subject to these requirements.

(4) For reporting, tracking, and recordkeeping when exceptions allow certain wastes or contaminated soil that do not meet the treatment standards to be land disposed: There are certain exemptions from the requirement that hazardous wastes or contaminated soil meet treatment standards before they can be land disposed. These include, but are not limited to case-by-case extensions under §268.5, disposal in a no-migration unit under §268.6, or a national capacity variance or case-by-case capacity variance under subpart C of this part. If a generator's waste is so exempt, then with the initial shipment of waste, the generator must send a one-time written notice to each land disposal facility receiving the waste. The notice must include the information indicated in column “268.7(a)(4)” of the Generator Paperwork Requirements Table below. If the waste changes, the generator must send a new notice to the receiving facility, and place a copy in their files.

(5) If a generator is managing and treating prohibited waste or contaminated soil in tanks, containers, or containment buildings regulated under 40 CFR 262.34 to meet applicable LDR treatment standards found at §268.40, the generator must develop and follow a written waste analysis plan which describes the procedures they will carry out to comply with the treatment standards. (Generators treating hazardous debris under the alternative treatment standards of Table 1, §268.45, however, are not subject to these waste analysis requirements.) The plan must be kept on site in the generator's records, and the following requirements must be met:

(i) The waste analysis plan must be based on a detailed chemical and physical analysis of a representative sample of the prohibited waste(s) being treated, and contain all information necessary to treat the waste(s) in accordance with the requirements of this part, including the selected testing frequency.

(ii) Such plan must be kept in the facility's on-site files and made available to inspectors.

(iii) Wastes shipped off-site pursuant to this paragraph must comply with the notification requirements of §268.7(a)(3).

(6) If a generator determines that the waste or contaminated soil is restricted based solely on his knowledge of the waste, all supporting data used to make this determination must be retained on-site in the generator's files. If a generator determines that the waste is restricted based on testing this waste or an extract developed using the test method 1311 in “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846, as referenced in §260.11 of this chapter, and all waste analysis data must be retained on-site in the generator's files.

(7) If a generator determines that he is managing a prohibited waste that is excluded from the definition of hazardous or solid waste or is exempted from Subtitle C regulation under 40 CFR 261.2 through 261.6 subsequent to the point of generation (including deactivated characteristic hazardous wastes managed in wastewater treatment systems subject to the Clean Water Act (CWA) as specified at 40 CFR 261.4(a)(2) or that are CWA-equivalent, or are managed in an underground injection well regulated by the SDWA), he must place a one-time notice describing such generation, subsequent exclusion from the definition of hazardous or solid waste or exemption from RCRA Subtitle C regulation, and the disposition of the waste, in the facility's on-site files.

(8) Generators must retain on-site a copy of all notices, certifications, waste analysis data, and other documentation produced pursuant to this section for at least three years from the date that the waste that is the subject of such documentation was last sent to on-site or off-site treatment, storage, or disposal. The three year record retention period is automatically extended during the course of any unresolved enforcement action regarding the regulated activity or as requested by the Administrator. The requirements of this paragraph apply to solid wastes even when the hazardous characteristic is removed prior to disposal, or when the waste is excluded from the definition of hazardous or solid waste under 40 CFR 261.2 through 261.6, or exempted from Subtitle C regulation, subsequent to the point of generation.

(9) If a generator is managing a lab pack containing hazardous wastes and wishes to use the alternative treatment standard for lab packs found at §268.42(c):

(i) With the initial shipment of waste to a treatment facility, the generator must submit a notice that provides the information in column “§268.7(a)(9)” in the Generator Paperwork Requirements Table of paragraph (a)(4) of this section, and the following certification. The certification, which must be signed by an authorized representative and must be placed in the generator's files, must say the following:

I certify under penalty of law that I personally have examined and am familiar with the waste and that the lab pack contains only wastes that have not been excluded under appendix IV to 40 CFR part 268 and that this lab pack will be sent to a combustion facility in compliance with the alternative treatment standards for lab packs at 40 CFR 268.42(c). I am aware that there are significant penalties for submitting a false certification, including the possibility of fine or imprisonment.

(ii) No further notification is necessary until such time that the wastes in the lab pack change, or the receiving facility changes, in which case a new notice and certification must be sent and a copy placed in the generator's file.

(iii) If the lab pack contains characteristic hazardous wastes (D001–D043), underlying hazardous constituents (as defined in §268.2(i)) need not be determined.

(iv) The generator must also comply with the requirements in paragraphs (a)(6) and (a)(7) of this section.

(10) Small quantity generators with tolling agreements pursuant to 40 CFR 262.20(e) must comply with the applicable notification and certification requirements of paragraph (a) of this section for the initial shipment of the waste subject to the agreement. Such generators must retain on-site a copy of the notification and certification, together with the tolling agreement, for at least three years after termination or expiration of the agreement. The three-year record retention period is automatically extended during the course of any unresolved enforcement action regarding the regulated activity or as requested by the Administrator.

(b) Treatment facilities must test their wastes according to the frequency specified in their waste analysis plans as required by 40 CFR 264.13 (for permitted TSDs) or 40 CFR 265.13 (for interim status facilities). Such testing must be performed as provided in paragraphs (b)(1), (b)(2) and (b)(3) of this section.

(1) For wastes or contaminated soil with treatment standards expressed in the waste extract (TCLP), the owner or operator of the treatment facility must test an extract of the treatment residues, using test method 1311 (the Toxicity Characteristic Leaching Procedure, described in “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846 as incorporated by reference in §260.11 of this chapter) to assure that the treatment residues extract meet the applicable treatment standards.

(2) For wastes or contaminated soil with treatment standards expressed as concentrations in the waste, the owner or operator of the treatment facility must test the treatment residues (not an extract of such residues) to assure that they meet the applicable treatment standards.

(3) A one-time notice must be sent with the initial shipment of waste or contaminated soil to the land disposal facility. A copy of the notice must be placed in the treatment facility's file.

(i) No further notification is necessary until such time that the waste or receiving facility change, in which case a new notice must be sent and a copy placed in the treatment facility's file.

(4) The treatment facility must submit a one-time certification signed by an authorized representative with the initial shipment of waste or treatment residue of a restricted waste to the land disposal facility. The certification must state:

I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification. Based on my inquiry of those individuals immediately responsible for obtaining this information, I believe that the treatment process has been operated and maintained properly so as to comply with the treatment standards specified in 40 CFR 268.40 without impermissible dilution of the prohibited waste. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment.

I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification and believe that it has been maintained and operated properly so as to comply with treatment standards specified in 40 CFR 268.49 without impermissible dilution of the prohibited wastes. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment.

(i) A copy of the certification must be placed in the treatment facility's on-site files. If the waste or treatment residue changes, or the receiving facility changes, a new certification must be sent to the receiving facility, and a copy placed in the file.

(ii) Debris excluded from the definition of hazardous waste under §261.3(f) of this chapter (i.e., debris treated by an extraction or destruction technology provided by Table 1, §268.45, and debris that the Director has determined does not contain hazardous waste), however, is subject to the notification and certification requirements of paragraph (d) of this section rather than the certification requirements of this paragraph.

(iii) For wastes with organic constituents having treatment standards expressed as concentration levels, if compliance with the treatment standards is based in whole or in part on the analytical detection limit alternative specified in §268.40(d), the certification, signed by an authorized representative, must state the following:

I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification. Based on my inquiry of those individuals immediately responsible for obtaining this information, I believe that the nonwastewater organic constituents have been treated by combustion units as specified in 268.42, Table 1. I have been unable to detect the nonwastewater organic constituents, despite having used best good-faith efforts to analyze for such constituents. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment.

(iv) For characteristic wastes that are subject to the treatment standards in §268.40 (other than those expressed as a method of treatment), or §268.49, and that contain underlying hazardous constituents as defined in §268.2(i); if these wastes are treated on-site to remove the hazardous characteristic; and are then sent off-site for treatment of underlying hazardous constituents, the certification must state the following:

I certify under penalty of law that the waste has been treated in accordance with the requirements of 40 CFR 268.40 or 268.49 to remove the hazardous characteristic. This decharacterized waste contains underlying hazardous constituents that require further treatment to meet treatment standards. I am aware that there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment.

(v) For characteristic wastes that contain underlying hazardous constituents as defined §268.2(i) that are treated on-site to remove the hazardous characteristic to treat underlying hazardous constituents to levels in §268.48 Universal Treatment Standards, the certification must state the following:

I certify under penalty of law that the waste has been treated in accordance with the requirements of 40 CFR 268.40 to remove the hazardous characteristic and that underlying hazardous constituents, as defined in §268.2(i) have been treated on-site to meet the §268.48 Universal Treatment Standards. I am aware that there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment.

(5) If the waste or treatment residue will be further managed at a different treatment, storage, or disposal facility, the treatment, storage, or disposal facility sending the waste or treatment residue off-site must comply with the notice and certification requirements applicable to generators under this section.

(6) Where the wastes are recyclable materials used in a manner constituting disposal subject to the provisions of §266.20(b) of this chapter regarding treatment standards and prohibition levels, the owner or operator of a treatment facility ( i.e. , the recycler) must, for the initial shipment of waste, prepare a one-time certification described in paragraph (b)(4) of this section, and a one-time notice which includes the information in paragraph (b)(3) of this section (except the manifest number). The certification and notification must be placed in the facility's on-site files. If the waste or the receiving facility changes, a new certification and notification must be prepared and placed in the on site files. In addition, the recycling facility must also keep records of the name and location of each entity receiving the hazardous waste-derived product.

(c) Except where the owner or operator is disposing of any waste that is a recyclable material used in a manner constituting disposal pursuant to 40 CFR 266.20(b), the owner or operator of any land disposal facility disposing any waste subject to restrictions under this part must:

(1) Have copies of the notice and certifications specified in paragraph (a) or (b) of this section.

(2) Test the waste, or an extract of the waste or treatment residue developed using test method 1311 (the Toxicity Characteristic Leaching Procedure, described in “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846 as incorporated by reference in §260.11 of this chapter), to assure that the wastes or treatment residues are in compliance with the applicable treatment standards set forth in subpart D of this part. Such testing must be performed according to the frequency specified in the facility's waste analysis plan as required by §264.13 or §265.13 of this chapter.

(d) Generators or treaters who first claim that hazardous debris is excluded from the definition of hazardous waste under §261.3(f) of this chapter (i.e., debris treated by an extraction or destruction technology provided by Table 1, §268.45, and debris that the EPA Regional Administrator (or his designated representative) or State authorized to implement part 268 requirements has determined does not contain hazardous waste) are subject to the following notification and certification requirements:

(1) A one-time notification, including the following information, must be submitted to the EPA Regional hazardous waste management division director (or his designated representative) or State authorized to implement part 268 requirements:

(i) The name and address of the Subtitle D facility receiving the treated debris;

(ii) A description of the hazardous debris as initially generated, including the applicable EPA Hazardous Waste Number(s); and

(iii) For debris excluded under §261.3(f)(1) of this chapter, the technology from Table 1, §268.45, used to treat the debris.

(2) The notification must be updated if the debris is shipped to a different facility, and, for debris excluded under §261.2(f)(1) of this chapter, if a different type of debris is treated or if a different technology is used to treat the debris.

(3) For debris excluded under §261.3(f)(1) of this chapter, the owner or operator of the treatment facility must document and certify compliance with the treatment standards of Table 1, §268.45, as follows:

(i) Records must be kept of all inspections, evaluations, and analyses of treated debris that are made to determine compliance with the treatment standards;

(ii) Records must be kept of any data or information the treater obtains during treatment of the debris that identifies key operating parameters of the treatment unit; and

(iii) For each shipment of treated debris, a certification of compliance with the treatment standards must be signed by an authorized representative and placed in the facility's files. The certification must state the following: “I certify under penalty of law that the debris has been treated in accordance with the requirements of 40 CFR 268.45. I am aware that there are significant penalties for making a false certification, including the possibility of fine and imprisonment.”

(e) Generators and treaters who first receive from EPA or an authorized state a determination that a given contaminated soil subject to LDRs as provided in §268.49(a) no longer contains a listed hazardous waste and generators and treaters who first determine that a contaminated soil subject to LDRs as provided in §268.49(a) no longer exhibits a characteristic of hazardous waste must:

(1) Prepare a one-time only documentation of these determinations including all supporting information; and,

(2) Maintain that information in the facility files and other records for a minimum of three years.

Editorial Note: ForFederal Registercitations affecting §268.7, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and on GPO Access.

§ 268.8 [Reserved]

(a) The initial generator of a solid waste must determine each EPA Hazardous Waste Number (waste code) applicable to the waste in order to determine the applicable treatment standards under subpart D of this part. This determination may be made concurrently with the hazardous waste determination required in §262.11 of this chapter. For purposes of part 268, the waste will carry the waste code for any applicable listed waste (40 CFR part 261, subpart D). In addition, where the waste exhibits a characteristic, the waste will carry one or more of the characteristic waste codes (40 CFR part 261, subpart C), except when the treatment standard for the listed waste operates in lieu of the treatment standard for the characteristic waste, as specified in paragraph (b) of this section. If the generator determines that their waste displays a hazardous characteristic (and is not D001 nonwastewaters treated by CMBST, RORGS, OR POLYM of §268.42, Table 1), the generator must determine the underlying hazardous constituents (as defined at §268.2(i)) in the characteristic waste.

(b) Where a prohibited waste is both listed under 40 CFR part 261, subpart D and exhibits a characteristic under 40 CFR part 261, subpart C, the treatment standard for the waste code listed in 40 CFR part 261, subpart D will operate in lieu of the standard for the waste code under 40 CFR part 261, subpart C, provided that the treatment standard for the listed waste includes a treatment standard for the constituent that causes the waste to exhibit the characteristic. Otherwise, the waste must meet the treatment standards for all applicable listed and characteristic waste codes.

(c) In addition to any applicable standards determined from the initial point of generation, no prohibited waste which exhibits a characteristic under 40 CFR part 261, subpart C may be land disposed unless the waste complies with the treatment standards under subpart D of this part.

(d) Wastes that exhibit a characteristic are also subject to §268.7 requirements, except that once the waste is no longer hazardous, a one-time notification and certification must be placed in the generator's or treater's on-site files. The notification and certification must be updated if the process or operation generating the waste changes and/or if the subtitle D facility receiving the waste changes.

(i) Name and address of the RCRA Subtitle D facility receiving the waste shipment; and

(ii) A description of the waste as initially generated, including the applicable EPA hazardous waste code(s), treatability group(s), and underlying hazardous constituents (as defined in §268.2(i)), unless the waste will be treated and monitored for all underlying hazardous constituents. If all underlying hazardous constituents will be treated and monitored, there is no requirement to list any of the underlying hazardous constituents on the notice.

(2) The certification must be signed by an authorized representative and must state the language found in §268.7(b)(4).

(i) If treatment removes the characteristic but does not meet standards applicable to underlying hazardous constituents, then the certification found in §268.7(b)(4)(iv) applies.

[55 FR 22688, June 1, 1990, as amended at 56 FR 3878, Jan. 31, 1991; 57 FR 37271, Aug. 18, 1992; 58 FR 29885, May 24, 1993; 59 FR 48045, Sept. 19, 1994; 60 FR 245, Jan. 3, 1995; 61 FR 15599, 15662, Apr. 8, 1996; 62 FR 26022, May 12, 1997; 64 FR 25415, May 11, 1999; 71 FR 16913, Apr. 4, 2006]

§§ 268.10-268.12 [Reserved]

In the case of any hazardous waste identified or listed under section 3001 after November 8, 1984, the Administrator shall make a land disposal prohibition determination within 6 months after the date of identification or listing.

(a) This section defines additional circumstances under which an otherwise prohibited waste may continue to be placed in a surface impoundment.

(b) Wastes which are newly identified or listed under section 3001 after November 8, 1984, and stored in a surface impoundment that is newly subject to subtitle C of RCRA as a result of the additional identification or listing, may continue to be stored in the surface impoundment for 48 months after the promulgation of the additional listing or characteristic, notwithstanding that the waste is otherwise prohibited from land disposal, provided that the surface impoundment is in compliance with the requirements of subpart F of part 265 of this chapter within 12 months after promulgation of the new listing or characteristic.

(c) Wastes which are newly identified or listed under section 3001 after November 8, 1984, and treated in a surface impoundment that is newly subject to subtitle C of RCRA as a result of the additional identification or listing, may continue to be treated in that surface impoundment, notwithstanding that the waste is otherwise prohibited from land disposal, provided that surface impoundment is in compliance with the requirements of subpart F of part 265 of this chapter within 12 months after the promulgation of the new listing or characteristic. In addition, if the surface impoundment continues to treat hazardous waste after 48 months from promulgation of the additional listing or characteristic, it must then be in compliance with §268.4.

(a) Effective August 23, 2005, the waste specified in 40 CFR part 261 as EPA Hazardous Waste Number K181, and soil and debris contaminated with this waste, radioactive wastes mixed with this waste, and soil and debris contaminated with radioactive wastes mixed with this waste are prohibited from land disposal.

(1) The wastes meet the applicable treatment standards specified in subpart D of this Part;

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable treatment standards established pursuant to a petition granted under §268.44;

(4) Hazardous debris has met the treatment standards in §268.40 or the alternative treatment standards in §268.45; or

(5) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to these wastes covered by the extension.

(c) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentrations in the waste extract of the waste, or the generator may use knowledge of the waste. If the waste contains regulated constituents in excess of the applicable subpart D levels, the waste is prohibited from land disposal, and all requirements of part 268 are applicable, except as otherwise specified.

(a) Effective August 11, 1997, the following wastes are prohibited from land disposal: the wastes specified in 40 CFR part 261 as EPA Hazardous Waste numbers F032, F034, and F035.

(b) Effective May 12, 1999, the following wastes are prohibited from land disposal: soil and debris contaminated with F032, F034, F035; and radioactive wastes mixed with EPA Hazardous waste numbers F032, F034, and F035.

(c) Between May 12, 1997 and May 12, 1999, soil and debris contaminated with F032, F034, F035; and radioactive waste mixed with F032, F034, and F035 may be disposed in a landfill or surface impoundment only if such unit is in compliance with the requirements specified in §268.5(h)(2) of this part.

(1) The wastes meet the applicable treatment standards specified in Subpart D of this part;

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable alternate treatment standards established pursuant to a petition granted under §268.44; or

(4) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to those wastes covered by the extension.

(e) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentrations in the waste extract or the waste, or the generator may use knowledge of the waste. If the waste contains constituents in excess of the applicable Universal Treatment Standard levels of §268.48 of this part, the waste is prohibited from land disposal, and all requirements of part 268 are applicable, except as otherwise specified.

(a) Effective November 8, 1988, the dioxin-containing wastes specified in 40 CFR 261.31 as EPA Hazardous Waste Nos. F020, F02l, F022, F023, F026, F027, and F028, are prohibited from land disposal unless the following condition applies:

(1) The F020–F023 and F026–F028 dioxin-containing waste is contaminated soil and debris resulting from a response action taken under section 104 or 106 of the Comprehensive Environmental Response, Compensation, and Liability Act of 1980 (CERCLA) or a corrective action taken under subtitle C of the Resource Conservation and Recovery Act (RCRA).

(b) Effective November 8, 1990, the F020–F023 and F026–F028 dioxin-containing wastes listed in paragraph (a)(1) of this section are prohibited from land disposal.

(c) Between November 8, 1988, and November 8, 1990, wastes included in paragraph (a)(1) of this section may be disposed in a landfill or surface impoundment only if such unit is in compliance with the requirements specified in §268.5(h)(2) and all other applicable requirements of parts 264 and 265 of this chapter.

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition; or

(3) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to those wastes covered by the extension.

(a) Effective December 26, 2000, the following wastes are prohibited from land disposal: any volumes of soil exhibiting the toxicity characteristic solely because of the presence of metals (D004—D011) and containing PCBs.

(1)(i) The wastes contain halogenated organic compounds in total concentration less than 1,000 mg/kg; and

(ii) The wastes meet the treatment standards specified in Subpart D of this part for EPA hazardous waste numbers D004—D011, as applicable; or

(2)(i) The wastes contain halogenated organic compounds in total concentration less than 1,000 mg/kg; and

(ii) The wastes meet the alternative treatment standards specified in §268.49 for contaminated soil; or

(3) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition; or

(4) The wastes meet applicable alternative treatment standards established pursuant to a petition granted under §268.44.

(a) Effective May 8, 2001, the wastes specified in 40 CFR part 261 as EPA Hazardous Wastes Numbers K174, and K175, soil and debris contaminated with these wastes, radioactive wastes mixed with these wastes, and soil and debris contaminated with radioactive wastes mixed with these wastes are prohibited from land disposal.

(1) The wastes meet the applicable treatment standards specified in subpart D of this part;

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable treatment standards established pursuant to a petition granted under §268.44;

(4) Hazardous debris has met the treatment standards in §268.40 or the alternative treatment standards in §268.45; or

(5) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to these wastes covered by the extension.

(c) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentrations in the waste extract or the waste, or the generator may use knowledge of the waste. If the waste contains regulated constituents in excess of the applicable levels of subpart D of this part, the waste is prohibited from land disposal, and all requirements of part 268 are applicable, except as otherwise specified.

(d) Disposal of K175 wastes that have complied with all applicable 40 CFR 268.40 treatment standards must also be macroencapsulated in accordance with 40 CFR 268.45 Table 1 unless the waste is placed in:

(1) A Subtitle C monofill containing only K175 wastes that meet all applicable 40 CFR 268.40 treatment standards; or

(2) A dedicated Subtitle C landfill cell in which all other wastes being co-disposed are at pH≤6.0.

(a) Effective August 24, 1998, the following wastes are prohibited from land disposal: the wastes specified in 40 CFR Part 261 as EPA Hazardous Waste numbers D004–D011 that are newly identified (i.e. wastes, soil, or debris identified as hazardous by the Toxic Characteristic Leaching Procedure but not the Extraction Procedure), and waste, soil, or debris from mineral processing operations that is identified as hazardous by the specifications at 40 CFR Part 261.

(b) Effective November 26, 1998, the following waste is prohibited from land disposal: Slag from secondary lead smelting which exhibits the Toxicity Characteristic due to the presence of one or more metals.

(c) Effective May 26, 2000, the following wastes are prohibited from land disposal: newly identified characteristic wastes from elemental phosphorus processing; radioactive wastes mixed with EPA Hazardous wastes D004–D011 that are newly identified (i.e., wastes, soil, or debris identified as hazardous by the Toxic Characteristic Leaching Procedure but not the Extraction Procedure); or mixed with newly identified characteristic mineral processing wastes, soil, or debris.

(d) Between May 26, 1998 and May 26, 2000, newly identified characteristic wastes from elemental phosphorus processing, radioactive waste mixed with D004–D011 wastes that are newly identified (i.e., wastes, soil, or debris identified as hazardous by the Toxic Characteristic Leaching Procedure but not the Extraction Procedure), or mixed with newly identified characteristic mineral processing wastes, soil, or debris may be disposed in a landfill or surface impoundment only if such unit is in compliance with the requirements specified in §268.5(h) of this part.

(1) The wastes meet the applicable treatment standards specified in subpart D of this part:

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable alternate treatment standards established pursuant to a petition granted under §268.44; or

(4) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to these wastes covered by the extension.

(f) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentration in the waste extract or the waste, or the generator may use knowledge of the waste. If the waste contains constituents (including underlying hazardous constituents in characteristic wastes) in excess of the applicable Universal Treatment Standard levels of §268.48 of this part, the waste is prohibited from land disposal, and all requirements of part 268 are applicable, except as otherwise specified.

(a) Effective February 8, 1999, the wastes specified in 40 CFR part 261 as EPA Hazardous Wastes Numbers K169, K170, K171, and K172, soils and debris contaminated with these wastes, radioactive wastes mixed with these hazardous wastes, and soils and debris contaminated with these radioactive mixed wastes, are prohibited from land disposal.

(1) The wastes meet the applicable treatment standards specified in Subpart D of this part;

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable treatment standards established pursuant to a petition granted under §268.44;

(4) Hazardous debris that have met treatment standards in §268.40 or in the alternative treatment standards in §268.45; or

(5) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to these wastes covered by the extension.

(c) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentrations in the waste extract or the waste, or the generator may use knowledge of the waste. If the waste contains constituents in excess of the applicable Universal Treatment Standard levels of §268.48, the waste is prohibited from land disposal, and all requirements of this part are applicable, except as otherwise specified.

(a) Effective May 20, 2002, the wastes specified in 40 CFR part 261 as EPA Hazardous Wastes Numbers K176, K177, and K178, and soil and debris contaminated with these wastes, radioactive wastes mixed with these wastes, and soil and debris contaminated with radioactive wastes mixed with these wastes are prohibited from land disposal.

(1) The wastes meet the applicable treatment standards specified in subpart D of this part;

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable treatment standards established pursuant to a petition granted under §268.44;

(4) Hazardous debris has met the treatment standards in §268.40 or the alternative treatment standards in §268.45; or

(5) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to these wastes covered by the extension.

(c) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentrations in the waste extract or the waste, or the generator may use knowledge of the waste. If the waste contains regulated constituents in excess of the applicable subpart D levels, the waste is prohibited from land disposal, and all requirements of this part are applicable, except as otherwise specified.

(a) Effective August 9, 1993, the wastes specified in 40 CFR 261.21 as D001 (and is not in the High TOC Ignitable Liquids Subcategory), and specified in §261.22 as D002, that are managed in systems other than those whose discharge is regulated under the Clean Water Act (CWA), or that inject in Class I deep wells regulated under the Safe Drinking Water Act (SDWA), or that are zero dischargers that engage in CWA-equivalent treatment before ultimate land disposal, are prohibited from land disposal. CWA-equivalent treatment means biological treatment for organics, alkaline chlorination or ferrous sulfate precipitation for cyanide, precipitation/sedimentation for metals, reduction of hexavalent chromium, or other treatment technology that can be demonstrated to perform equally or greater than these technologies.

(b) Effective February 10, 1994, the wastes specified in 40 CFR 261.21 as D001 (and is not in the High TOC Ignitable Liquids Subcategory), and specified in §261.22 as D002, that are managed in systems defined in 40 CFR 144.6(e) and 146.6(e) as Class V injection wells, that do not engage in CWA-equivalent treatment before injection, are prohibited from land disposal.

(a) Effective December 19, 1994, the wastes specified in 40 CFR 261.32 as EPA Hazardous Waste numbers K141, K142, K143, K144, K145, K147, K148, K149, K150, and K151 are prohibited from land disposal. In addition, debris contaminated with EPA Hazardous Waste numbers F037, F038, K107–K112, K117, K118, K123–K126, K131, K132, K136, U328, U353, U359, and soil and debris contaminated with D012–D043, K141–K145, and K147–K151 are prohibited from land disposal. The following wastes that are specified in 40 CFR 261.24, Table 1 as EPA Hazardous Waste numbers: D012, D013, D014, D015, D016, D017, D018, D019, D020, D021, D022, D023, D024, D025, D026, D027, D028, D029, D030, D031, D032, D033, D034, D035, D036, D037, D038, D039, D040, D041, D042, D043 that are not radioactive, or that are managed in systems other than those whose discharge is regulated under the Clean Water Act (CWA), or that are zero dischargers that do not engage in CWA-equivalent treatment before ultimate land disposal, or that are injected in Class I deep wells regulated under the Safe Drinking Water Act (SDWA), are prohibited from land disposal. CWA-equivalent treatment means biological treatment for organics, alkaline chlorination or ferrous sulfate precipitation for cyanide, precipitation/ sedimentation for metals, reduction of hexavalent chromium, or other treatment technology that can be demonstrated to perform equally or better than these technologies.

(b) On September 19, 1996, radioactive wastes that are mixed with D018–D043 that are managed in systems other than those whose discharge is regulated under the Clean Water Act (CWA), or that inject in Class I deep wells regulated under the Safe Drinking Water Act (SDWA), or that are zero dischargers that engage in CWA-equivalent treatment before ultimate land disposal, are prohibited from land disposal. CWA-equivalent treatment means biological treatment for organics, alkaline chlorination or ferrous sulfate precipitation for cyanide, precipitation/ sedimentation for metals, reduction of hexavalent chromium, or other treatment technology that can be demonstrated to perform equally or greater than these technologies. Radioactive wastes mixed with K141–K145, and K147–K151 are also prohibited from land disposal. In addition, soil and debris contaminated with these radioactive mixed wastes are prohibited from land disposal.

(c) Between December 19, 1994 and September 19, 1996, the wastes included in paragraphs (b) of this section may be disposed in a landfill or surface impoundment, only if such unit is in compliance with the requirements specified in §268.5(h)(2) of this Part.

(d) The requirements of paragraphs (a), (b), and (c) of this section do not apply if:

(1) The wastes meet the applicable treatment standards specified in Subpart D of this part;

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable alternate treatment standards established pursuant to a petition granted under §268.44;

(4) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to these wastes covered by the extension.

(e) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentrations in the waste extract or the waste, or the generator may use knowledge of the waste. If the waste contains constituents in excess of the applicable Subpart D levels, the waste is prohibited from land disposal, and all requirements of part 268 are applicable, except as otherwise specified.

(a) On July 8, 1996, the wastes specified in 40 CFR 261.32 as EPA Hazardous Waste numbers K156–K159, and K161; and in 40 CFR 261.33 as EPA Hazardous Waste numbers P127, P128, P185, P188–P192, P194, P196–P199, P201–P205, U271, U278–U280, U364, U367, U372, U373, U387, U389, U394, U395, U404, and U409–U411 are prohibited from land disposal. In addition, soil and debris contaminated with these wastes are prohibited from land disposal.

(b) On July 8, 1996, the wastes identified in 40 CFR 261.23 as D003 that are managed in systems other than those whose discharge is regulated under the Clean Water Act (CWA), or that inject in Class I deep wells regulated under the Safe Drinking Water Act (SDWA), or that are zero dischargers that engage in CWA-equivalent treatment before ultimate land disposal, are prohibited from land disposal. This prohibition does not apply to unexploded ordnance and other explosive devices which have been the subject of an emergency response. (Such D003 wastes are prohibited unless they meet the treatment standard of DEACT before land disposal (see §268.40)).

(c) On September 21, 1998, the wastes specified in 40 CFR 261.32 as EPA Hazardous Waste number K088 are prohibited from land disposal. In addition, soil and debris contaminated with these wastes are prohibited from land disposal.

(d) On April 8, 1998, radioactive wastes mixed with K088, K156–K159, K161, P127, P128, P185, P188–P192, P194, P196–P199, P201–P205, U271, U278–U280, U364, U367, U372, U373, U387, U389, U394, U395, U404, and U409–U411 are prohibited from land disposal. In addition, soil and debris contaminated with these radioactive mixed wastes are prohibited from land disposal.

(e) Between July 8, 1996, and April 8, 1998, the wastes included in paragraphs (a), (c), and (d) of this section may be disposed in a landfill or surface impoundment, only if such unit is in compliance with the requirements specified in §268.5(h)(2).

(f) The requirements of paragraphs (a), (b), (c), and (d) of this section do not apply if:

(1) The wastes meet the applicable treatment standards specified in Subpart D of this part;

(2) Persons have been granted an exemption from a prohibition pursuant to a petition under §268.6, with respect to those wastes and units covered by the petition;

(3) The wastes meet the applicable alternate treatment standards established pursuant to a petition granted under §268.44;

(4) Persons have been granted an extension to the effective date of a prohibition pursuant to §268.5, with respect to these wastes covered by the extension.

(g) To determine whether a hazardous waste identified in this section exceeds the applicable treatment standards specified in §268.40, the initial generator must test a sample of the waste extract or the entire waste, depending on whether the treatment standards are expressed as concentrations in the waste extract or the waste, or the generator may use knowledge of the waste. If the waste contains constituents in excess of the applicable Subpart D levels, the waste is prohibited from land disposal, and all requirements of this part 268 are applicable, except as otherwise specified.

[61 FR 15663, Apr. 8, 1996, as amended at 61 FR 33683, June 28, 1996; 62 FR 1997, Jan. 14, 1997; 62 FR 32979, June 17, 1997; 62 FR 37699, July 14, 1997; 63 FR 51264, Sept. 24, 1998]

(a) A prohibited waste identified in the table “Treatment Standards for Hazardous Wastes” may be land disposed only if it meets the requirements found in the table. For each waste, the table identifies one of three types of treatment standard requirements:

(1) All hazardous constituents in the waste or in the treatment residue must be at or below the values found in the table for that waste (“total waste standards”); or

(2) The hazardous constituents in the extract of the waste or in the extract of the treatment residue must be at or below the values found in the table (“waste extract standards”); or

(3) The waste must be treated using the technology specified in the table (“technology standard”), which are described in detail in §268.42, Table 1—Technology Codes and Description of Technology-Based Standards.

(b) For wastewaters, compliance with concentration level standards is based on maximums for any one day, except for D004 through D011 wastes for which the previously promulgated treatment standards based on grab samples remain in effect. For all nonwastewaters, compliance with concentration level standards is based on grab sampling. For wastes covered by the waste extract standards, the test Method 1311, the Toxicity Characteristic Leaching Procedure found in “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846, as incorporated by reference in §260.11, must be used to measure compliance. An exception is made for D004 and D008, for which either of two test methods may be used: Method 1311, or Method 1310B, the Extraction Procedure Toxicity Test. For wastes covered by a technology standard, the wastes may be land disposed after being treated using that specified technology or an equivalent treatment technology approved by the Administrator under the procedures set forth in §268.42(b).

(c) When wastes with differing treatment standards for a constituent of concern are combined for purposes of treatment, the treatment residue must meet the lowest treatment standard for the constituent of concern.

(d) Notwithstanding the prohibitions specified in paragraph (a) of this section, treatment and disposal facilities may demonstrate (and certify pursuant to 40 CFR 268.7(b)(5)) compliance with the treatment standards for organic constituents specified by a footnote in the table “Treatment Standards for Hazardous Wastes” in this section, provided the following conditions are satisfied:

(1) The treatment standards for the organic constituents were established based on incineration in units operated in accordance with the technical requirements of 40 CFR part 264, subpart O, or based on combustion in fuel substitution units operating in accordance with applicable technical requirements;

(2) The treatment or disposal facility has used the methods referenced in paragraph (d)(1) of this section to treat the organic constituents; and

(3) The treatment or disposal facility may demonstrate compliance with organic constituents if good-faith analytical efforts achieve detection limits for the regulated organic constituents that do not exceed the treatment standards specified in this section by an order of magnitude.

(e) For characteristic wastes (D001–D043) that are subject to treatment standards in the following table “Treatment Standards for Hazardous Wastes,” and are not managed in a wastewater treatment system that is regulated under the Clean Water Act (CWA), that is CWA-equivalent, or that is injected into a Class I nonhazardous deep injection well, all underlying hazardous constituents (as defined in §268.2(i)) must meet Universal Treatment Standards, found in §268.48, Table Universal Treatment Standards, prior to land disposal as defined in §268.2(c) of this part.

(f) The treatment standards for F001–F005 nonwastewater constituents carbon disulfide, cyclohexanone, and/or methanol apply to wastes which contain only one, two, or three of these constituents. Compliance is measured for these constituents in the waste extract from test Method 1311, the Toxicity Characteristic Leaching Procedure found in “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods”, EPA Publication SW–846, as incorporated by reference in §260.11. If the waste contains any of these three constituents along with any of the other 25 constituents found in F001–F005, then compliance with treatment standards for carbon disulfide, cyclohexanone, and/or methanol are not required.

(g) Between August 26, 1996 and March 4, 1999 the treatment standards for the wastes specified in 40 CFR 261.32 as EPA Hazardous Waste numbers K156–K161; and in 40 CFR 261.33 as EPA Hazardous Waste numbers P127, P128, P185, P188–P192, P194, P196–P199, P201–P205, U271, U277–U280, U364–U367, U372, U373, U375–U379, U381–U387, U389–U396, U400–U404, U407, and U409–U411; and soil contaminated with these wastes; may be satisfied by either meeting the constituent concentrations presented in the table “Treatment Standards for Hazardous Wastes” in this section, or by treating the waste by the following technologies: combustion, as defined by the technology code CMBST at §268.42 Table 1, for nonwastewaters; and, biodegradation as defined by the technology code BIODG, carbon adsorption as defined by the technology code CARBN, chemical oxidation as defined by the technology code CHOXD, or combustion as defined as technology code CMBST at §268.42 Table 1, for wastewaters.

(h) Prohibited D004–D011 mixed radioactive wastes and mixed radioactive listed wastes containing metal constituents, that were previously treated by stabilization to the treatment standards in effect at that time and then put into storage, do not have to be re-treated to meet treatment standards in this section prior to land disposal.

(j) Effective September 4, 1998, the treatment standards for the wastes specified in 40 CFR 261.33 as EPA Hazardous Waste numbers P185, P191, P192, P197, U364, U394, and U395 may be satisfied by either meeting the constituent concentrations presented in the table “Treatment Standards for Hazardous Wastes” in this section, or by treating the waste by the following technologies: combustion, as defined by the technology code CMBST at §268.42 Table 1 of this Part, for nonwastewaters; and, biodegradation as defined by the technology code BIODG, carbon adsorption as defined by the technology code CARBN, chemical oxidation as defined by the technology code CHOXD, or combustion as defined as technology code CMBST at §268.42 Table 1 of this Part, for wastewaters.

Treatment Standards For Hazardous Wastes

[Note: NA means not applicable]

Waste code	Waste description and treatment/Regulatory subcategory¹	Regulated hazardous constituent		Wastewaters	Nonwastewaters
Waste code	Waste description and treatment/Regulatory subcategory¹	Common name	CAS² number	Concentration³in mg/L; or Technology Code⁴	Concentration⁵in mg/kg unless noted as “mg/L TCLP”; or Technology Code⁴
D001⁹	Ignitable Characteristic Wastes, except for the §261.21(a)(1) High TOC Subcategory.	NA	NA	DEACT and meet §268.48 standards⁸; or RORGS; or CMBST	DEACT and meet §268.48 standards⁸; or RORGS; or CMBST
	High TOC Ignitable Characteristic Liquids Subcategory based on 40 CFR 261.21(a)(1)—Greater than or equal to 10% total organic carbon. (Note: This subcategory consists of nonwastewaters only.)	NA	NA	NA	RORGS; CMBST; or POLYM
D002⁹	Corrosive Characteristic Wastes.	NA	NA	DEACT and meet §268.48 standards⁸	DEACT and meet §268.48 standards⁸
D002, D004, D005, D006, D007, D008, D009, D010, D011	Radioactive high level wastes generated during the reprocessing of fuel rods. (Note: This subcategory consists of nonwastewaters only.)	Corrosivity (pH) Arsenic Barium Cadmium Chromium (Total) Lead Mercury Selenium Silver	NA 7440–38–2 7440–39–3 7440–43–9 7440–47–3 7439–92–1 7439–97–6 7782–49–2 7440–22–4	NA NA NA NA NA NA NA NA NA	HLVIT HLVIT HLVIT HLVIT HLVIT HLVIT HLVIT HLVIT HLVIT
D003⁹	Reactive Sulfides Subcategory based on 261.23(a)(5).	NA	NA	DEACT	DEACT
	Explosives Subcategory based on 261.23(a)(6),(7), and (8).	NA	NA	DEACT and meet §268.48 standards⁸	DEACT and meet §268.48 standards⁸
	Unexploded ordnance and other explosive devices which have been the subject of an emergency response.	NA	NA	DEACT	DEACT
	Other Reactives Subcategory based on 261.23(a)(1).	NA	NA	DEACT and meet §268.48 standards⁸	DEACT and meet §268.48 standards⁸
	Water Reactive Subcategory based on 261.23(a)(2), (3), and (4). (Note: This subcategory consists of nonwastewaters only).	NA	NA	NA	DEACT and meet §268.48 standards⁸
	Reactive Cyanides Subcategory based on 261.23(a)(5).	Cyanides (Total)⁷	57–12–5	Reserved	590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
D004⁹	Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for arsenic based on the toxicity characteristic leaching procedure (TCLP) in SW846.	Arsenic	7440–38–2	1.4 and meet §268.48 standards⁸	5.0 mg/L TCLP and meet §268.48 standards⁸
D005⁹	Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for barium based on the toxicity characteristic leaching procedure (TCLP) in SW846.	Barium	7440–39–3	1.2 and meet §268.48 standards⁸	21 mg/L TCLP and meet §268.48 standards⁸
D006⁹	Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for cadmium based on the toxicity characteristic leaching procedure (TCLP) in SW846.	Cadmium	7440–43–9	0.69 and meet §268.48 standards⁸	0.11 mg/L TCLP and meet §268.48 standards⁸
	Cadmium Containing Batteries Subcategory. (Note: This subcategory consists of nonwastewaters only).	Cadmium	7440–43–9	NA	RTHRM
	Radioactively contaminated cadmium containing batteries. (Note:This subcategory consists of nonwastewaters only)	Cadmium	7440–43–9	NA	Macroencapsulation in accordance with 40 CFR 268.45.
D007⁹	Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for chromium based on the toxicity characteristic leaching procedure (TCLP) in SW846.	Chromium (Total)	7440–47–3	2.77 and meet §268.48 standards⁸	0.60 mg/L TCLP and meet §268.48 standards⁸
D008⁹	Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for lead based on the toxicity characteristic leaching procedure (TCLP) in SW846.	Lead	7439–92–1	0.69 and meet §268.48 standards⁸	0.75 mg/L TCLP and meet §268.48 standards⁸
	Lead Acid Batteries Subcategory (Note: This standard only applies to lead acid batteries that are identified as RCRA hazardous wastes and that are not excluded elsewhere from regulation under the land disposal restrictions of 40 CFR 268 or exempted under other EPA regulations (see 40 CFR 266.80). This subcategory consists of nonwastewaters only.)	Lead	7439–92–1	NA	RLEAD
	Radioactive Lead Solids Subcategory (Note: These lead solids include, but are not limited to, all forms of lead shielding and other elemental forms of lead. These lead solids do not include treatment residuals such as hydroxide sludges, other wastewater treatment residuals, or incinerator ashes that can undergo conventional pozzolanic stabilization, nor do they include organo-lead materials that can be incinerated and stabilized as ash. This subcategory consists of nonwastewaters only.)	Lead	7439–92–1	NA	MACRO
D009⁹	Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for mercury based on the toxicity characteristic leaching procedure (TCLP) in SW846; and contain greater than or equal to 260 mg/kg total mercury that also contain organics and are not incinerator residues. (High Mercury-Organic Subcategory)	Mercury	7439–97–6	NA	IMERC; OR RMERC
	Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for mercury based on the toxicity characteristic leaching procedure (TCLP) in SW846; and contain greater than or equal to 260 mg/kg total mercury that are inorganic, including incinerator residues and residues from RMERC. (High Mercury-Inorganic Subcategory)	Mercury	7439–97–6	NA	RMERC
	Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for mercury based on the toxicity characteristic leaching procedure (TCLP) in SW846; and contain less than 260 mg/kg total mercury and that are residues from RMERC only. (Low Mercury Subcategory)	Mercury	7439–97–6	NA	0.20 mg/L TCLP and meet §268.48 standards⁸
	All other nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for mercury based on the toxicity characteristic leaching procedure (TCLP) in SW846; and contain less than 260 mg/kg total mercury and that are not residues from RMERC. (Low Mercury Subcategory)	Mercury	7439–97–6	NA	0.025 mg/L TCLP and meet §268.48 standards⁸
	All D009 wastewaters.	Mercury	7439–97–6	0.15 mg/L TCLP and meet §268.48 standards⁸	NA
	Elemental mercury contaminated with radioactive materials. (Note: This subcategory consists of nonwastewaters only.)	Mercury	7439–97–6	NA	AMLGM
	Hydraulic oil contaminated with Mercury Radioactive Materials Subcategory. (Note: This subcategory consists of nonwastewaters only.)	Mercury	7439–97–6	NA	IMERC
	Radioactively contaminated mercury containing batteries.(Note:This subcategory consists of nonwastewaters only)	Mercury	7439–97–6	NA	Macroencapsulation in accordance with 40 CFR 268.45.
D010⁹	Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for selenium based on the toxicity characteristic leaching procedure (TCLP) in SW846.	Selenium	7782–49–2	0.82 and meet §268.48 standards⁸	5.7 mg/L TCLP and meet §268.48 standards⁸
D011⁹	Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for silver based on the toxicity characteristic leaching procedure (TCLP) in SW846.	Silver	7440–22–4	0.43 and meet §268.48 standards⁸	0.14 mg/L TCLP and meet §268.48 standards⁸
	Radioactively contaminated silver containing batteries.Note:This subcategory consists of nonwastewaters only)	Silver	7440–22–4	NA	Macroencapsulation in accordance with 40 CFR 268.45.
D012⁹	Wastes that are TC for Endrin based on the TCLP in SW846 Method 1311.	Endrin	72–20–8	BIODG; or CMBST	0.13 and meet §268.48 standards⁸
		Endrin aldehyde	7421–93–4	BIODG; or CMBST	0.13 and meet §268.48 standards⁸
D013⁹	Wastes that are TC for Lindane based on the TCLP in SW846 Method 1311.	alpha-BHC	319–84–6	CARBN; or CMBST	0.066 and meet §268.48 standards⁸
		beta-BHC	319–85–7	CARBN; or CMBST	0.066 and meet §268.48 standards⁸
		delta-BHC	319–86–8	CARBN; or CMBST	0.066 and meet §268.48 standards⁸
		gamma-BHC (Lindane)	58–89–9	CARBN; or CMBST	0.066 and meet §268.48 standards⁸
D014⁹	Wastes that are TC for Methoxychlor based on the TCLP in SW846 Method 1311.	Methoxychlor	72–43–5	WETOX or CMBST	0.18 and meet §268.48 standards⁸
D015⁹	Wastes that are TC for Toxaphene based on the TCLP in SW846 Method 1311.	Toxaphene	8001–35–2	BIODG or CMBST	2.6 and meet §268.48 standards⁸
D016⁹	Wastes that are TC for 2,4-D (2,4-Dichlorophenoxyacetic acid) based on the TCLP in SW846 Method 1311.	2,4,-D (2,4-Dichlorophenoxyacetic acid)	94–75–7	CHOXD, BIODG, or CMBST	10 and meet §268.48 standards⁸
D017⁹	Wastes that are TC for 2,4,5-TP (Silvex) based on the TCLP in SW846 Method 1311.	2,4,5-TP (Silvex)	93–72–1	CHOXD or CMBST	7.9 and meet §268.48 standards⁸
D018⁹	Wastes that are TC for Benzene based on the TCLP in SW846 Method 1311.	Benzene	71–43–2	0.14 and meet §268.48 standards⁸	10 and meet §268.48 standards⁸
D019⁹	Wastes that are TC for Carbon tetrachloride based on the TCLP in SW846 Method 1311.	Carbon tetrachloride	56–23–5	0.057 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D020⁹	Wastes that are TC for Chlordane based on the TCLP in SW846 Method 1311.	Chlordane (alpha and gamma isomers)	57–74–9	0.0033 and meet §268.48 standards⁸	0.26 and meet §268.48 standards⁸
D021⁹	Wastes that are TC for Chlorobenzene based on the TCLP in SW846 Method 1311.	Chlorobenzene	108–90–7	0.057 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D022⁹	Wastes that are TC for Chloroform based on the TCLP in SW846 Method 1311.	Chloroform	67–66–3	0.046 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D023⁹	Wastes that are TC for o-Cresol based on the TCLP in SW846 Method 1311.	o-Cresol	95–48–7	0.11 and meet §268.48 standards⁸	5.6 and meet §268.48 standards⁸
D024⁹	Wastes that are TC for m-Cresol based on the TCLP in SW846 Method 1311.	m-Cresol (difficult to distinguish from p-cresol)	108–39–4	0.77 and meet §268.48 standards⁸	5.6 and meet §268.48 standards⁸
D025⁹	Wastes that are TC for p-Cresol based on the TCLP in SW846 Method 1311.	p-Cresol (difficult to distinguish from m-cresol)	106–44–5	0.77 and meet §268.48 standards⁸	5.6 and meet §268.48 standards⁸
D026⁹	Wastes that are TC for Cresols (Total) based on the TCLP in SW846 Method 1311.	Cresol-mixed isomers (Cresylic acid) (sum of o-, m-, and p-cresol concentrations)	1319–77–3	0.88 and meet §268.48 standards⁸	11.2 and meet §268.48 standards⁸
D027⁹	Wastes that are TC for p-Dichlorobenzene based on the TCLP in SW846 Method 1311.	p-Dichlorobenzene (1,4-Dichlorobenzene)	106–46–7	0.090 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D028⁹	Wastes that are TC for 1,2-Dichloroethane based on the TCLP in SW846 Method 1311.	1,2-Dichloroethane	107–06–2	0.21 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D029⁹	Wastes that are TC for 1,1-Dichloroethylene based on the TCLP in SW846 Method 1311.	1,1-Dichloroethylene	75–35–4	0.025 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D030⁹	Wastes that are TC for 2,4-Dinitrotoluene based on the TCLP in SW846 Method 1311.	2,4-Dinitrotoluene	121–14–2	0.32 and meet §268.48 standards⁸	140 and meet §268.48 standards⁸
D031⁹	Wastes that are TC for Heptachlor based on the TCLP in SW846 Method 1311.	Heptachlor	76–44–8	0.0012 and meet §268.48 standards⁸	0.066 and meet §268.48 standards⁸
		Heptachlor epoxide	1024–57–3	0.016 and meet §268.48 standards⁸	0.066 and meet §268.48 standards⁸
D032⁹	Wastes that are TC for Hexachlorobenzene based on the TCLP in SW846 Method 1311.	Hexachlorobenzene	118–74–1	0.055 and meet §268.48 standards⁸	10 and meet §268.48 standards⁸
D033⁹	Wastes that are TC for Hexachlorobutadiene based on the TCLP in SW846 Method 1311.	Hexachlorobutadiene	87–68–3	0.055 and meet §268.48 standards⁸	5.6 and meet §268.48 standards⁸
D034⁹	Wastes that are TC for Hexachloroethane based on the TCLP in SW846 Method 1311.	Hexachloroethane	67–72–1	0.055 and meet §268.48 standards⁸	30 and meet §268.48 standards⁸
D035⁹	Wastes that are TC for Methyl ethyl ketone based on the TCLP in SW846 Method 1311.	Methyl ethyl ketone	78–93–3	0.28 and meet §268.48 standards⁸	36 and meet §268.48 standards⁸
D036⁹	Wastes that are TC for Nitrobenzene based on the TCLP in SW846 Method 1311.	Nitrobenzene	98–95–3	0.068 and meet §268.48 standards⁸	14 and meet §268.48 standards⁸
D037⁹	Wastes that are TC for Pentachlorophenol based on the TCLP in SW846 Method 1311.	Pentachlorophenol	87–86–5	0.089 and meet §268.48 standards⁸	7.4 and meet §268.48 standards⁸
D038⁹	Wastes that are TC for Pyridine based on the TCLP in SW846 Method 1311.	Pyridine	110–86–1	0.014 and meet §268.48 standards⁸	16 and meet §268.48 standards⁸
D039⁹	Wastes that are TC for Tetrachloroethylene based on the TCLP in SW846 Method 1311.	Tetrachloroethylene	127–18–4	0.056 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D040⁹	Wastes that are TC for Trichloroethylene based on the TCLP in SW846 Method 1311.	Trichloroethylene	79–01–6	0.054 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
D041⁹	Wastes that are TC for 2,4,5-Trichlorophenol based on the TCLP in SW846 Method 1311.	2,4,5-Trichlorophenol	95–95–4	0.18 and meet §268.48 standards⁸	7.4 and meet §268.48 standards⁸
D042⁹	Wastes that are TC for 2,4,6-Trichlorophenol based on the TCLP in SW846 Method 1311.	2,4,6-Trichlorophenol	88–06–2	0.035 and meet §268.48 standards⁸	7.4 and meet §268.48 standards⁸
D043⁹	Wastes that are TC for Vinyl chloride based on the TCLP in SW846 Method 1311.	Vinyl chloride	75–01–4	0.27 and meet §268.48 standards⁸	6.0 and meet §268.48 standards⁸
F001, F002, F003, F004, & F005	F001, F002, F003, F004 and/or F005 solvent wastes that contain any combination of one or more of the following spent solvents: acetone, benzene, n-butyl alcohol, carbon disulfide, carbon tetrachloride, chlorinated fluorocarbons, chlorobenzene, o-cresol, m-cresol, p-cresol, cyclohexanone, o-dichlorobenzene, 2-ethoxyethanol, ethyl acetate, ethyl benzene, ethyl ether, isobutyl alcohol, methanol, methylene chloride, methyl ethyl ketone, methyl isobutyl ketone, nitrobenzene, 2-nitropropane, pyridine, tetrachloroethylene, toluene, 1,1,1-trichloroethane, 1,1,2-trichloroethane, 1,1,2-trichloro-1,2,2-trifluoroethane, trichloroethylene, trichlorofluoromethane, and/or xylenes [except as specifically noted in other subcategories]. See further details of these listings in §261.31.	Acetone Benzene n-Buthyl alcohol Carbon disulfide Carbon tetrachloride Chlorobenzene o-Cresol m-Cresol (difficult to distinguish from p-cresol) p-Cresol (difficult to distinguish from m-cresol) Cresol-mixed isomers (Cresylic acid) (sum of o-, m-, and p-cresol concentrations)	67–64–1 71–43–2 71–36–3 75–15–0 56–23–5 108–90–7 95–48–7 108–39–4 106–44–5 1319–77–3	0.28 0.14 5.6 3.8 0.057 0.057 0.11 0.77 0.77 0.88	160 10 2.6 NA 6.0 6.0 5.6 5.6 5.6 11.2
		Cyclohexanone	108–94–1	0.36	NA
		o-Dichlorobenzene	95–50–1	0.088	6.0
		Ethyl acetate	141–78–6	0.34	33
		Ethyl benzene	100–41–4	0.057	10
		Ethyl ether	60–29–7	0.12	160
		Isobutyl alcohol	78–83–1	5.6	170
		Methanol	67–56–1	5.6	NA
		Methylene chloride	75–9–2	0.089	30
		Methyl ethyl ketone	78–93–3	0.28	36
		Methyl isobutyl ketone	108–10–1	0.14	33
		Nitrobenzene	98–95–3	0.068	14
		Pyridine	110–86–1	0.014	16
		Tetrachloroethylene	127–18–4	0.056	6.0
		Toluene	108–88–3	0.080	10
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
		1,1,2-Trichloroethane	79–00–5	0.054	6.0
		1,1,2-Trichloro-1,2,2-trifluoroethane	76–13–1	0.057	30
		Trichloroethylene	79–01–6	0.054	6.0
		Trichlorofluoromethane	75–69–4	0.020	30
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
	F003 and/or F005 solvent wastes that contain any combination of one or more of the following three solvents as the only listed F001–5 solvents: carbon disulfide, cyclohexanone, and/or methanol. (formerly 268.41(c))	Carbon disulfide Cyclohexanone Methanol	75–15–0 108–94–1 67–56–1	3.8 0.36 5.6	4.8 mg/L TCLP 0.75 mg/L TCLP 0.75 mg/L TCLP
	F005 solvent waste containing 2-Nitropropane as the only listed F001–5 solvent.	2-Nitropropane	79–46–9	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
	F005 solvent waste containing 2-Ethoxyethanol as the only listed F001–5 solvent.	2-Ethoxyethanol	110–80–5	BIODG; or CMBST	CMBST
F006	Wastewater treatment sludges from electroplating operations except from the following processes: (1) Sulfuric acid anodizing of aluminum; (2) tin plating on carbon steel; (3) zinc plating (segregated basis) on carbon steel; (4) aluminum or zinc-aluminum plating on carbon steel; (5) cleaning/stripping associated with tin, zinc and aluminum plating on carbon steel; and (6) chemical etching and milling of aluminum.	Cadmium Chromium (Total) Cyanides (Total)⁷ Cyanides (Amenable)⁷ Lead Nickel Silver	7440–43–9 7440–47–3 57–12–5 57–12–5 7439–92–1 7440–02–0 7440–22–4	0.69 2.77 1.2 0.86 0.69 3.98 NA	0.11 mg/L TCLP 0.60 mg/L TCLP 590 30 0.75 mg/L TCLP 11 mg/L TCLP 0.14 mg/L TCLP
F007	Spent cyanide plating bath solutions from electroplating operations.	Cadmium Chromium (Total)	7440–43–9 7440–47–3	NA 2.77	0.11 mg/L TCLP 0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Silver	7440–22–4	NA	0.14 mg/L TCLP
F008	Plating bath residues from the bottom of plating baths from electroplating operations where cyanides are used in the process.	Cadmium Chromium (Total) Cyanides (Total)⁷	7440–43–9 7440–47–3 57–12–5	NA 2.77 1.2	0.11 mg/L TCLP 0.60 mg/L TCLP 590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Silver	7440–22–4	NA	0.14 mg/L TCLP
F009	Spent stripping and cleaning bath solutions from electroplating operations where cyanides are used in the process.	Cadmium Chromium (Total)	7440–43–9 7440–47–3	NA 2.77	0.11 mg/L TCLP 0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Silver	7440–22–4	NA	0.14 mg/L TCLP
F010	Quenching bath residues from oil baths from metal heat treating operations where cyanides are used in the process.	Cyanides (Total)⁷ Cyanides (Amenable)⁷	57–12–5 57–12–5	1.2 0.86	590 NA
F011	Spent cyanide solutions from salt bath pot cleaning from metal heat treating operations.	Cadmium Chromium (Total)	7440–43–9 7440–47–3	NA 2.77	0.11 mg/L TCLP 0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Silver	7440–22–4	NA	0.14 mg/L TCLP
F012	Quenching wastewater treatment sludges from metal heat treating operations where cyanides are used in the process.	Cadmium Chromium (Total)	7440–43–9 7440–47–3	NA 2.77	0.11 mg/L TCLP 0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Silver	7440–22–4	NA	0.14 mg/L TCLP
F019	Wastewater treatment sludges from the chemical conversion coating of aluminum except from zirconium phosphating in aluminum can washing when such phosphating is an exclusive conversion coating process.	Chromium (Total) Cyanides (Total)⁷ Cyanides (Amendable)⁷	7440–47–3 57–12–5 57–12–5	2.77 1.2 0.86	0.60 mg/L TCLP 590 30
F020, F021, F022, F023, F026	Wastes (except wastewater and spent carbon from hydrogen chloride purification) from the production or manufacturing use (as a reactant, chemical intermediate, or component in a formulating process) of: (1) tri- or tetrachlorophenol, or of intermediates used to produce their pesticide derivatives, excluding wastes from the production of Hexachlorophene from highly purified, 2,4,5-trichlorophenol (F020); (2) pentachlorophenol, or of intermediates used to produce its derivatives (i.e., F021); (3) tetra-, penta-, or hexachlorobenzenes under alkaline conditions (i.e., F022); and from the production of materials on equipment previously used for the production or manufacturing use (as a reactant, chemical intermediate, or component in a formulating process) of: (1) tri- or tetrachlorophenols, excluding wastes from equipment used only for the production of Hexachlorophene from highly purified 2,4,5-trichlorophenol (F023); (2) tetra- penta, or hexachlorobenzenes under alkaline conditions (i.e., F026).	HxCDDs (All Hexachlorodibenzo-p-dioxins) Hx CDFs (All Hexachlorodibenzofurans) PeCDDs (All Pentachlorodibenzo-p-dioxins) PeCDFs (All Pentachlorodibenzofurans) Pentachlorophenol TCDDs (All Tetrachlorodibenzo-p-dioxins) TCDFs (All Tetrachlorodibenzofurans) 2,4,5-Trichlorophenol 2,4-6-Trichlorophenol 2,3,4,6-Tetrachlorophenol	NA NA NA NA 87–86–5 NA NA 95–95–4 88–06–2 58–90–2	0.000063 0.000063 0.000063 0.000035 0.089 0.000063 0.000063 0.18 0.035 0.030	0.001 0.001 0.001 0.001 7.4 0.001 0.001 7.4 7.4 7.4
F024	Process wastes, including but not limited to, distillation residues, heavy ends, tars, and reactor clean-out wastes, from the production of certain chlorinated aliphatic hydrocarbons by free radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon chain lengths ranging from one to and including five, with varying amounts and positions of chlorine substitution. (This listing does not include wastewaters, wastewater treatment sludges, spent catalysts, and wastes listed in §261.31 or §261.32).	All F024 wastes 2-Chloro-1,3-butadiene 3-Chloropropylene 1,1-Dichloroethane 1,2-Dichloroethane 1,2-Dichloropropane cis-1,3-Dichloropropylene trans-1-3-Dichloropropylene bis(2-Ethylhexyl)phthalate Hexachloroethane Chromium (Total) Nickel	NA 126–99–8 107–05–1 75–34–3 107–06–2 78–87–5 10061–01–5 10061–02–6 117–81–7 67–72–1 7440–47–3 7440–02–0	CMBST¹¹ 0.057 0.036 0.059 0.21 0.85 0.036 0.036 0.28 0.055 2.77 3.98	CMBST¹¹ 0.28 30 6.0 6.0 18 18 18 28 30 0.60 mg/L TCLP 11 mg/L TCLP
F025	Condensed light ends from the production of certain chlorinated aliphatic hydrocarbons, by free radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon chain lengths ranging from one to and including five, with varying amounts and positions of chlorine substitution. F025—Light Ends Subcategory	Carbon tetrachloride Chloroform 1,2-Dichloroethane 1,1-Dichloroethylene Methylene chloride 1,1,2-Trichloroethane Trichloroethylene Vinyl chloride	56–23–5 67–66–3 107–06–2 75–35–4 75–9–2 79–00–5 79–01–6 75–01–4	0.057 0.046 0.21 0.025 0.089 0.054 0.054 0.027	6.0 6.0 6.0 6.0 30 6.0 6.0 6.0
	Spent filters and filter aids, and spent desiccant wastes from the production of certain chlorinated aliphatic hydrocarbons, by free radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon chain lengths ranging from one to and including five, with varying amounts and positions of chlorine substitution. F025—Spent Filters/Aids and Desiccants Subcategory	Carbon tetrachloride Chloroform Hexachlorobenzene Hexachlorobutadiene Hexachloroethane Methylene chloride 1,1,2-Trichloroethane Trichloroethylene Vinyl chloride	56–23–5 67–66–3 118–74–1 87–68–3 67–72–1 75–9–2 79–00–5 79–01–6 75–01–4	0.057 0.046 0.055 0.055 0.055 0.089 0.054 0.054 0.27	6.0 6.0 10 5.6 30 30 6.0 6.0 6.0
F027	Discarded unused formulations containing tri-, tetra-, or pentachlorophenol or discarded unused formulations containing compounds derived from these chlorophenols. (This listing does not include formulations containing hexachlorophene synthesized from prepurified 2,4,5-trichlorophenol as the sole component.)	HxCDDs (All Hexachlorodibenzo-p-dioxins) HxCDFs (All Hexachlorodibenzofurans) PeCDDs (All Pentachlorodibenzo-p-dioxins) PeCDFs (All Pentachlorodibenzofurans) Pentachlorophenol TCDDs (All Tetrachlorodibenzo-p-dioxins) TCDFs (All Tetrachlorodibenzofurans) 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,3,4,6-Tetrachlorophenol	NA NA NA NA 87–86–5 NA NA 95–95–4 88–06–2 58–90–2	0.000063 0.000063 0.000063 0.000035 0.089 0.000063 0.000063 0.18 0.035 0.030	0.001 0.001 0.001 0.001 7.4 0.001 0.001 7.4 7.4 7.4
F028	Residues resulting from the incineration or thermal treatment of soil contaminated with EPA Hazardous Wastes Nos. F020, F021, F023, F026, and F027.	HxCDDs (All Hexachlorodibenzo-p-dioxins) HxCDFs (All Hexachlorodibenzofurans) PeCDDs (All Pentachlorodibenzo-p-dioxins)	NA NA NA	0.000063 0.000063 0.000063	0.001 0.001 0.001
		PeCDFs (All Pentachlorodibenzofurans)	NA	0.000035	0.001
		Pentachlorophenol	87–86–5	0.089	7.4
		TCDDs (All Tetrachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		TCDFs (All Tetrachlorodibenzofurans)	NA	0.000063	0.001
		2,4,5-Trichlorophenol	95–95–4	0.18	7.4
		2,4,6-Trichlorophenol	88–06–2	0.035	7.4
		2,3,4,6-Tetrachlorophenol	58–90–2	0.030	7.4
F032	Wastewaters (except those that have not come into contact with process contaminants), process residuals, preservative drippage, and spent formulations from wood preserving processes generated at plants that currently use or have previously used chlorophenolic formulations (except potentially cross-contaminated wastes that have had the F032 waste code deleted in accordance with §261.35 of this chapter or potentially cross-contaminated wastes that are otherwise currently regulated as hazardous wastes (i.e., F034 or F035), and where the generator does not resume or initiate use of chlorophenolic formulations). This listing does not include K001 bottom sediment sludge from the treatment of wastewater from wood preserving processes that use creosote and/or penta-chlorophenol.	Acenaphthene Anthracene Benz(a)anthracene Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene) Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene) Benzo(a)pyrene Chrysene Dibenz(a,h) anthracene 2-4-Dimethyl phenol Fluorene Hexachlorodibenzo-p-dioxins Hexachlorodibenzofurans	83–32–9 120–12–7 56–55–3 205–99–2 207–08–9 50–32–8 218–01–9 53–70–3 105–67–9 86–73–7 NA NA	0.059 0.059 0.059 0.11 0.11 0.061 0.059 0.055 0.036 0.059 0.000063, or CMBST¹¹ 0.000063, or CMBST¹¹	3.4 3.4 3.4 6.8 6.8 3.4 3.4 8.2 14 3.4 0.001, or CMBST¹¹ 0.001, or CMBST¹¹
		Indeno (1,2,3-c,d) pyrene	193–39–5	0.0055	3.4
		Naphthalene	91–20–3	0.059	5.6
		Pentachlorodibenzo-p-dioxins	NA	0.000063, or CMBST¹¹	0.001, or CMBST¹¹
		Pentachlorodibenzofurans	NA	0.00035, or CMBST¹¹	0.001, or CMBST¹¹
		Pentachlorophenol	87–86–5	0.089	7.4
		Phenanthrene	85–01–8	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Pyrene	129–00–0	0.067	8.2
		Tetrachlorodibenzo-p-dioxins	NA	0.000063, or CMBST¹¹	0.001, or CMBST¹¹
		Tetrachlorodibenzofurans	NA	0.000063, or CMBST¹¹	0.001, or CMBST¹¹
		2,3,4,6-Tetrachlorophenol	58–90–2	0.030	7.4
		2,4,6-Trichlorophenol	88–06–2	0.035	7.4
		Arsenic	7440–38–2	1.4	5.0 mg/L TCLP
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
F034	Wasteswaters (except those that have not come into contact with process contaminants), process residuals, preservative drippage, and spent formulations from wood preserving processes generated at plants that use creosote formulations. This listing does not include K001 bottom sediment sludge from the treatment of wastewater from wood preserving processes that use creosote and/or pentachlorophenol.	Acenaphthene Anthracene Benz(a)anthracene Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene) Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene) Benzo(a)pyrene	83–32–9 120–12–7 56–55–3 205–99–2 207–08–9 50–32–8	0.059 0.059 0.059 0.11 0.11 0.061	3.4 3.4 3.4 6.8 6.8 3.4
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Fluorene	86–73–7	0.059	3.4
		Indeno(1,2,3-c,d)pyrene	193–39–5	0.0055	3.4
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–8	0.059	5.6
		Pyrene	129–00–0	0.067	8.2
		Arsenic	7440–38–2	1.4	5.0 mg/L TCLP
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
F035	Wastewaters (except those that have not come into contact with process contaminants), process residuals, preservative drippage, and spent formulations from wood preserving processes generated at plants that use inorganic preservatives containing arsenic or chromium. This listing does not include K001 bottom sediment sludge from the treatment of wastewater from wood preserving processes that use creosote and/or pentachlorophenol.	Arsenic Chromium (Total)	7440–38–2 7440–47–3	1.4 2.77	5.0 mg/L TCLP 0.60 mg/L TCLP
F037	Petroleum refinery primary oil/water/solids separation sludge—Any sludge generated from the gravitational separation of oil/water/solids during the storage or treatment of process wastewaters and oily cooling wastewaters from petroleum refineries. Such sludges include, but are not limited to, those generated in: oil/water/solids separators; tanks and impoundments; ditches and other conveyances; sumps; and stormwater units receiving dry weather flow. Sludge generated in stormwater units that do not receive dry weather flow, sludges generated from non-contact once-through cooling waters segregated for treatment from other process or oily cooling waters, sludges generated in aggressive biological treatment units as defined in §261.31(b)(2) (including sludges generated in one or more additional units after wastewaters have been treated in aggressive biological treatment units) and K051 wastes are not included in this listing.	Acenaphthene Anthracene Benzene Benz(a)anthracene Benzo(a)pyrene bis(2-Ethylhexyl) phthalate Chrysene Di-n-butyl phthalate Ethylbenzene Fluorene Naphthalene Phenanthrene Phenol Pyrene Toluene Xylenes-mixed isomers (sum of o, m-, and p-xylene concentrations)	83–32–9 120–12–7 71–43–2 56–55–3 50–32–8 117–81–7 218–01–9 84–74–2 100–41–4 86–73–7 91–20–3 85–01–8 108–95–2 129–00–0 108–88–3 1330–20–7	0.059 0.059 0.14 0.059 0.061 0.28 0.059 0.057 0.057 0.059 0.059 0.059 0.039 0.067 0.080 0.32	NA 3.4 10 3.4 3.4 28 3.4 28 10 NA 5.6 5.6 6.2 8.2 10 30
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Lead	7439–92–1	0.69	NA
		Nickel	7440–02–0	NA	11 mg/L TCLP
F038	Petroleum refinery secondary (emulsified) oil/water/solids separation sludge and/or float generated from the physical and/or chemical separation of oil/water/solids in process wastewaters and oily cooling wastewaters from petroleum refineries. Such wastes include, but are not limited to, all sludges and floats generated in: induced air floatation (IAF) units, tanks and impoundments, and all sludges generated in DAF units. Sludges generated in stormwater units that do not receive dry weather flow, sludges generated from non-contact once-through cooling waters segregated for treatment from other process or oily cooling waters, sludges and floats generated in aggressive biological treatment units as defined in §261.31(b)(2) (including sludges and floats generated in one or more additional units after wastewaters have been treated in aggressive biological units) and F037, K048, and K051 are not included in this listing.	Benzene Benzo(a)pyrene bis(2-Ethylhexyl) phthalate Chrysene Di-n-butyl phthalate Ethylbenzene Fluorene Naphthalene Phenanthrene Phenol Pyrene Toluene Xylenes-mixed isomers (sum of o, m-, and p-xylene concentrations) Chromium (Total) Cyanides (Total)⁷ Lead	71–43–2 50–32–8 117–81–7 218–01–9 84–74–2 100–41–4 86–73–7 91–20–3 85–01–8 108–95–2 129–00–0 108–88–3 1330–20–7 7440–47–3 57–12–5 7439–92–1	0.14 0.061 0.28 0.059 0.057 0.057 0.059 0.059 0.059 0.039 0.067 0.080 0.32 2.77 1.2 0.69	10 3.4 28 3.4 28 10 NA 5.6 5.6 6.2 8.2 10 30 0.60 mg/L TCLP 590 NA
		Nickel	7440–02–0	NA	11 mg/L TCLP
F039	Leachate (liquids that have percolated through land disposed wastes) resulting from the disposal of more than one restricted waste classified as hazardous under subpart D of this part. (Leachate resulting from the disposal of one or more of the following EPA Hazardous Wastes and no other Hazardous Wastes retains its EPA Hazardous Waste Number(s): F020, F021, F022, F026, F027, and/or F028.)	Acenaphthylene Acenaphthene Acetone Acetonitrile Acetophenone 2-Acetylaminofluorene Acrolein	208–96–8 83–32–9 67–64–1 75–05–8 96–86–2 53–96–3 107–02–8	0.059 0.059 0.28 5.6 0.010 0.059 0.29	3,4 3.4 160 NA 9.7 140 NA
		Acrylonitrile	107–13–1	0.24	84
		Aldrin	309–00–2	0.021	0.066
		4-Aminobiphenyl	92–67–1	0.13	NA
		Aniline	62–53–3	0.81	14
		o-Anisidine (2-methoxyaniline)	90-04-0	0.010	0.66
		Anthracene	120–12–7	0.059	3.4
		Aramite	140–57–8	0.36	NA
		alpha-BHC	319–84–6	0.00014	0.066
		beta-BHC	319–85–7	0.00014	0.066
		delta-BHC	319–86–8	0.023	0.066
		gamma-BHC	58–89–9	0.0017	0.066
		Benzene	71–43–2	0.14	10
		Benz(a)anthracene	56–55–3	0.059	3.4
		Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	205–99–2	0.11	6.8
		Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene)	207–08–9	0.11	6.8
		Benzo(g,h,i)perylene	191–24–2	0.0055	1.8
		Benzo(a)pyrene	50–32–8	0.061	3.4
		Bromodichloromethane	75–27–4	0.35	15
		Methyl bromide (Bromomethane)	74–83–9	0.11	15
		4-Bromophenyl phenyl ether	101–55–3	0.055	15
		n-Butyl alcohol	71–36–3	5.6	2.6
		Butyl benzyl phthalate	85–68–7	0.017	28
		2-sec-Buty-4,6-dinitrophenol (Dinoseb)	88–85–7	0.066	2.5
		Carbon disulfide	75–15–0	3.8	NA
		Carbon tetrachloride	56–23–5	0.057	6.0
		Chlordane (alpha and gamma isomers)	57–74–9	0.0033	0.26
		p-Chloroaniline	106–47–8	0.46	16
		Chlorobenzene	108–90–7	0.057	6.0
		Chlorobenzilate	510–15–6	0.10	NA
		2-Chloro-1,3-butadiene	126–99–8	0.057	NA
		Chlorodibromomethane	124–48–1	0.057	15
		Chloroethane	75–00–3	0.27	6.0
		bis(2-Chloroethoxy)methane	111–91–1	0.036	7.2
		bis(2-Chloroethyl)ether	111–44–4	0.033	6.0
		Chloroform	67–66–3	0.046	6.0
		bis(2-Chloroisopropyl)ether	39638–32–9	0.055	7.2
		p-Chloro-m-cresol	59–50–7	0.018	14
		Chloromethane (Methyl chloride)	74–87–3	0.19	30
		2-Chloronaphthalene	91–58–7	0.055	5.6
		2-Chlorophenol	95–57–8	0.044	5.7
		3-Chloropropylene	107–05–1	0.036	30
		Chrysene	218–01–9	0.059	3.4
		o-Cresol	95–48–7	0.11	5.6
		p-Cresidine	120-71-8	0.010	0.66
		m-Cresol (difficult to distinguish from p-cresol)	108–39–4	0.77	5.6
		p-Cresol (difficult to distinguish from m-cresol)	106–44–5	0.77	5.6
		Cyclohexanone	108–94–1	0.36	NA
		1,2-Dibromo-3-chloropropane	96–12–8	0.11	15
		Ethylene dibromide (1,2-Dibromoethane)	106–93–4	0.028	15
		Dibromomethane	74–95–3	0.11	15
		2,4-D (2,4-Dichlorophenoxyacetic acid)	94–75–7	0.72	10
		o,p′-DD	53–19-0	0.023	0.087
		p,p′-DDD	72–54–8	0.023	0.087
		o,p′-DDE	3424–82–6	0.031	0.087
		p,p′-DDE	72–55–9	0.031	0.087
		o,p′-DDT	789–02–6	0.0039	0.087
		p,p′-DDT	50–29–3	0.0039	0.087
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Dibenz(a,e)pyrene	192–65–4	0.061	NA
		m-Dichlorobenzene	541–73–1	0.036	6.0
		o-Dichlorobenzene	95–50–1	0.088	6.0
		p-Dichlorobenzene	106–46–7	0.090	6.0
		Dichlorodifluoromethane	75–71–8	0.23	7.2
		1,1-Dichloroethane	75–34–3	0.059	6.0
		1,2-Dichloroethane	107–06–2	0.21	6.0
		1,1-Dichloroethylene	75–35–4	0.025	6.0
		trans-1,2-Dichloroethylene	156–60–5	0.054	30
		2,4-Dichlorophenol	120–83–2	0.044	14
		2,6-Dichlorophenol	87–65–0	0.044	14
		1,2-Dichloropropane	78–87–5	0.85	18
		cis-1,3-Dichloropropylene	10061–01–5	0.036	18
		trans-1,3-Dichloropropylene	10061–02–6	0.036	18
		Dieldrin	60–57–1	0.017	0.13
		Diethyl phthalate	84–66–2	0.20	28
		2,4-Dimethylaniline (2,4-xylidine)	95-68-1	0.010	0.66
		2-4-Dimethyl phenol	105–67–9	0.036	14
		Dimethyl phthalate	131–11–3	0.047	28
		Di-n-butyl phthalate	84–74–2	0.057	28
		1,4-Dinitrobenzene	100–25–4	0.32	2.3
		4,6-Dinitro-o-cresol	534–52–1	0.28	160
		2,4-Dinitrophenol	51–28–5	0.12	160
		2,4-Dinitrotoluene	121–14–2	0.32	140
		2,6-Dinitrotoluene	606–20–2	0.55	28
		Di-n-octyl phthalate	117–84–0	0.017	28
		Di-n-propylnitrosamine	621–64–7	0.40	14
		1,4-Dioxane	123–91–1	12.0	170
		Diphenylamine (difficult to distinguish from diphenylnitrosamine)	122–39–4	0.92	NA
		Diphenylnitrosamine (difficult to distinguish from diphenylamine)	86–30–6	0.92	NA
		1,2-Diphenylhydrazine	122–66–7	0.087	NA
		Disulfoton	298–04–4	0.017	6.2
		Endosulfan I	939–98–8	0.023	0.066
		Endosulfan II	33213–6–5	0.029	0.13
		Endosulfan sulfate	1031–07–8	0.029	0.13
		Endrin	72–20–8	0.0028	0.13
		Endrin aldehyde	7421–93–4	0.025	0.13
		Ethyl acetate	141–78–6	0.34	33
		Ethyl cyanide (Propanenitrile)	107–12–0	0.24	360
		Ethyl benzene	100–41–4	0.057	10
		Ethyl ether	60–29–7	0.12	160
		bis(2-Ethylhexyl) phthalate	117–81–7	0.28	28
		Ethyl methacrylate	97–63–2	0.14	160
		Ethylene oxide	75–21–8	0.12	NA
		Famphur	52–85–7	0.017	15
		Fluoranthene	206–44–0	0.068	3.4
		Fluorene	86–73–7	0.059	3.4
		Heptachlor	76–44–8	0.0012	0.066
		Heptachlor epoxide	1024–57–3	0.016	0.066
		1,2,3,4,6,7,8-Heptachlorodibenzo- p -dioxin (1,2,3,4,6,7,8-HpCDD)	35822–46–9	0.000035	0.0025
		1, 2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-HpCDF)	67562–39–4	0.000035	0.0025
		1,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-HpCDF)	55673–89–7	0.000035	0.0025
		Hexachlorobenzene	118–74–1	0.055	10
		Hexachlorobutadiene	87–68–3	0.055	5.6
		Hexachlorocyclopentadiene	77–47–4	0.057	2.4
		HxCDDs (All Hexachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		HxCDFs (All Hexachlorodibenzofurans)	NA	0.000063	0.001
		Hexachloroethane	67–72–1	0.055	30
		Hexachloropropylene	1888–71–7	0.035	30
		Indeno (1,2,3-c,d) pyrene	193–39–5	0.0055	3.4
		Indomethane	74–88–4	0.019	65
		Isobutyl alcohol	78–83–1	5.6	170
		Isodrin	465-73-6	0.021	0.066
		Isosafrole	120–58–1	0.081	2.6
		Kepone	143–50–8	0.0011	0.13
		Methacylonitrile	126–98–7	0.24	84
		Methanol	67–56–1	5.6	NA
		Methapyrilene	91–80–5	0.081	1.5
		Methoxychlor	72–43–5	0.25	0.18
		3-Methylcholanthrene	56–49–5	0.0055	15
		4,4-Methylene bis(2-chloroaniline)	101–14–4	0.50	30
		Methylene chloride	75–09–2	0.089	30
		Methyl ethyl ketone	78–93–3	0.28	36
		Methyl isobutyl ketone	108–10–1	0.14	33
		Methyl methacrylate	80–62–6	0.14	160
		Methyl methanesulfonate	66–27–3	0.018	NA
		Methyl parathion	298–00–0	0.014	4.6
		Naphthalene	91–20–3	0.059	5.6
		2-Naphthylamine	91–59–8	0.52	NA
		p-Nitroaniline	100–01–6	0.028	28
		Nitrobenzene	98–95–3	0.068	14
		5-Nitro-o-toluidine	99–55–8	0.32	28
		p-Nitrophenol	100–02–7	0.12	29
		N-Nitrosodiethylamine	55–18–5	0.40	28
		N-Nitrosodimethylamine	62–75–9	0.40	NA
		N-Nitroso-di-n-butylamine	924–16–3	0.40	17
		N-Nitrosomethylethylamine	10595–95–6	0.40	2.3
		N-Nitrosomorpholine	59–89–2	0.40	2.3
		N-Nitrosopiperidine	100–75–4	0.013	35
		N-Nitrosopyrrolidine	930–55–2	0.013	35
		1,2,3,4,6,7,8,9-Octachlorodibenzo- p -dioxin (OCDD)	3268–87–9	0.000063	0.005
		1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)	39001–02–0	0.000063	0.005
		Parathion	56–38–2	0.014	4.6
		Total PCBs (sum of all PCB isomers, or all Aroclors)	1336–36–3	0.10	10
		Pentachlorobenzene	608–93–5	0.055	10
		PeCDDs (All Pentachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		PeCDFs (All Pentachlorodibenzofurans)	NA	0.000035	0.001
		Pentachloronitrobenzene	82–68–8	0.055	4.8
		Pentachlorophenol	87–86–5	0.089	7.4
		Phenacetin	62–44–2	0.081	16
		Phenanthrene	85–01–8	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		2,4-Dimethylaniline (2,4-xylidine)	108-45-2	0.010	0.66
		Phorate	298–02–2	0.021	4.6
		Phthalic anhydride	85–44–9	0.055	NA
		Pronamide	23950–58–5	0.093	1.5
		Pyrene	129–00–0	0.067	8.2
		Pyridine	110–86–1	0.014	16
		Safrole	94–59–7	0.081	22
		Silvex (2,4,5-TP)	93–72–1	0.72	7.9
		2,4,5-T	93–76–5	0.72	7.9
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	14
		TCDDs (All Tetrachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		TCDFs (All Tetrachlorodibenzofurans)	NA	0.000063	0.001
		1,1,1,2-Tetrachloroethane	630–20–6	0.057	6.0
		1,1,2,2-Tetrachloroethane	79–34–6	0.057	6.0
		Tetrachloroethylene	127–18–4	0.056	6.0
		2,3,4,6-Tetrachlorophenol	58–90–2	0.030	7.4
		Toluene	108–88–3	0.080	10
		Toxaphene	8001–35–2	0.0095	2.6
		Bromoform (Tribromomethane)	75–25–2	0.63	15
		1,2,4-Trichlorobenzene	120–82–1	0.055	19
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
		1,1,2-Trichloroethane	79–00–5	0.054	6.0
		Trichloroethylene	79–01–6	0.054	6.0
		Trichlorofluoromethane	75–69–4	0.020	30
		2,4,5-Trichlorophenol	95–95-4	0.18	7.4
		2,4,6-Trichlorophenol	88–06–2	0.035	7.4
		1,2,3-Trichloropropane	96–18–4	0.85	30
		1,1,2-Trichloro-1,2,2-trifluoroethane	76–13–1	0.057	30
		tris(2,3-Dibromopropyl) phosphate	126–72–7	0.11	NA
		Vinyl chloride	75–01–4	0.27	6.0
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Antimony	7440–36–0	1.9	1.15 mg/L TCLP
		Arsenic	7440–38–2	1.4	5.0 mg/L TCLP
		Barium	7440–39–3	1.2	21 mg/L TCLP
		Beryllium	7440–41–7	0.82	NA
		Cadmium	7440–43–9	0.69	0.11 mg/L TCLP
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Cyanides (Amenable)⁷	57–12–5	0.86	NA
		Fluoride	16984–48–8	35	NA
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Mercury	7439–97–6	0.15	0.25 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Selenium	7782–49–2	0.82	5.7 mg/L TCLP
		Silver	7440–22–4	0.43	0.14 mg/L TCLP
		Sulfide	8496–25–8	14	NA
		Thallium	7440–28–0	1.4	NA
		Vanadium	7440–62–2	4.3	NA
K001	Bottom sediment sludge from the treatment of wastewaters from wood preserving processes that use creosote and/or pentachlorophenol.	Naphthalene Pentachlorophenol Phenanthrene Pyrene	91–20–3 87–86–5 85–01–8 129–00–0	0.059 0.089 0.059 0.067	5.6 7.4 5.6 8.2
		Toluene	108–88–3	0.080	10
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
K002	Wastewater treatment sludge from the production of chrome yellow and orange pigments.	Chromium (Total) Lead	7440–47–3 7439–92–1	2.77 0.69	0.60 mg/L TCLP 0.75 mg/L TCLP
K003	Wastewater treatment sludge from the production of molybdate orange pigments.	Chromium (Total) Lead	7440–47–3 7439–92–1	2.77 0.69	0.60 mg/L TCLP 0.75 mg/L TCLP
K004	Wastewater treatment sludge from the production of zinc yellow pigments.	Chromium (Total) Lead	7440–47–3 7439–92–1	2.77 0.69	0.60 mg/L TCLP 0.75 mg/L TCLP
K005	Wastewater treatment sludge from the production of chrome green pigments.	Chromium (Total) Lead Cyanides (Total)⁷	7440–47–3 7439–92–1 57–12–5	2.77 0.69 1.2	0.60 mg/L TCLP 0.75 mg/L TCLP 590
K006	Wastewater treatment sludge from the production of chrome oxide green pigments (anhydrous).	Chromium (Total) Lead	7440–47–3 7439–92–1	2.77 0.69	0.60 mg/L TCLP 0.75 mg/L TCLP
	Wastewater treatment sludge from the production of chrome oxide green pigments (hydrated).	Chromium (Total) Lead	7440–47–3 7439–92–1	2.77 0.69	0.60 mg/L TCLP NA
K007	Wastewater treatment sludge from the production of iron blue pigments.	Chromium (Total) Lead Cyanides (Total)⁷	7440–47–3 7439–92–1 57–12–5	2,77 0.69 1.2	0.60 mg/L TCLP 0.75 mg/L TCLP 590
K008	Oven residue from the production of chrome oxide green pigments.	Chromium (Total) Lead	7440–47–3 7439–92–1	2.77 0.69	0.60 mg/L TCLP 0.75 mg/L TCLP
K009	Distillation bottoms from the production of acetaldehyde from ethylene.	Chloroform	67–66–3	0.046	6.0
K010	Distillation side cuts from the production of acetaldehyde from ethylene.	Chloroform	67–66–3	0.046	6.0
K011	Bottom stream from the wastewater stripper in the production of acrylonitrile.	Acetonitrile Acrylonitrile	75–05–8 107–13–1	5.6 0.24	38 84
		Acrylamide	79–06–1	19	23
		Benzene	71–43–2	0.14	10
		Cyanide (Total)	57–12–5	1.2	590
K013	Bottom stream from the acetonitrile column in the production of acrylonitrile.	Acetonitrile Acrylonitrile	75–05–8 107–13–1	5.6 0.24	38 84
		Acrylamide	79–06–1	19	23
		Benzene	71–43–2	0.14	10
		Cyanide (Total)	57–12–5	1.2	590
K014	Bottoms from the acetonitrile purification column in the production of acrylonitrile.	Acetonitrile Acrylonitrile	75–05–8 107–13–1	5.6 0.24	38 84
		Acrylamide	79–06–1	19	23
		Benzene	71–43–2	0.14	10
		Cyanide (Total)	57–12–5	1.2	590
K015	Still bottoms from the distillation of benzyl chloride.	Anthracene Benzal chloride	120–12–7 98–87–3	0.059 0.055	3.4 6.0
		Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	205–99–2	0.11	6.8
		Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene)	207–08–9	0.11	6.8
		Phenanthrene	85–01–8	0.059	5.6
		Toluene	108–88–3	0.080	10
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
K016	Heavy ends or distillation residues from the production of carbon tetrachloride.	Hexachlorobenzene Hexachlorobutadiene	118–74–1 87–68–3	0.055 0.055	10 5.6
		Hexachlorocyclopentadiene	77–47–4	0.057	2.4
		Hexachloroethane	67–72–1	0.055	30
		Tetrachloroethylene	127–18–4	0.056	6.0
K017	Heavy ends (still bottoms) from the purification column in the production of epichlorohydrin.	bis(2-Chloroethyl)ether 1,2-Dichloropropane 1,2,3-Trichloropropane	111–44–4 78–87–5 96–18–4	0.033 0.85 0.85	6.0 18 30
K018	Heavy ends from the fractionation column in ethyl chloride production.	Chloroethane Chloromethane 1,1-Dichloroethane	75–00–3 74–87–3 75–34–3	0.27 0.19 0.059	6.0 NA 6.0
		1,2-Dichloroethane	107–06–2	0.21	6.0
		Hexachlorobenzene	118–74–1	0.055	10
		Hexachlorobutadiene	87–68–3	0.055	5.6
		Hexachloroethane	67–72–1	0.055	30
		Pentachloroethane	76–01–7	NA	6.0
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
K019	Heavy ends from the distillation of ethylene dichloride in ethylene dichloride production.	bis(2-Chloroethyl)ether Chlorobenzene	111–44–4 108–90–7	0.033 0.057	6.0 6.0
		Chloroform	67–66–3	0.046	6.0
		p-Dichlorobenzene	106–46–7	0.090	NA
		1,2-Dichloroethane	107–06–2	0.21	6.0
		Fluorene	86–73–7	0.059	NA
		Hexachloroethane	67–72–1	0.055	30
		Nephthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–8	0.059	5.6
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	NA
		Tetrachloroethylene	127–18–4	0.056	6.0
		1,2,4-Trichlorobenzene	120–82–1	0.055	19
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
K020	Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer production.	1,2-Dichloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene	107–06–2 79–34–6 127–18–4	0.21 0.057 0.056	6.0 6.0 6.0
K021	Aqueous spent antimony catalyst waste from fluoromethanes production.	Carbon tetrachloride Chloroform Antimony	56–23–5 67–66–3 7440–36–0	0.057 0.046 1.9	6.0 6.0 1.15 mg/L TCLP
K022	Distillation bottoms tars from the production of phenol/acetone from cumene.	Toluene Acetophenone	108–88–3 96–86–2	0.080 0.010	10 9.7
		Diphenylamine (difficult to distinguish from diphenylnitrosamine)	122–39–4	0.92	13
		Diphenylnitrosamine (difficult to distinguish from diphenylamine)	86–30–6	0.92	13
		Phenol	108–95–2	0.039	6.2
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
K023	Distillation light ends from the production of phthalic anhydride from naphthalene.	Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	100–21–0	0.055	28
		Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	85–44–9	0.055	28
K024	Distillation bottoms from the production of phthalic anhydride from naphthalene.	Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	100–21–0	0.055	28
		Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	85–44–9	0.055	28
K025	Distillation bottoms from the production of nitrobenzene by the nitration of benzene.	NA	NA	LLEXT fb SSTRP fb CARBN; or CMBST	CMBST
K026	Stripping still tails from the production of methyl ethyl pyridines.	NA	NA	CMBST	CMBST
K027	Centrifuge and distillation residues from toluene diisocyanate production.	NA	NA	CARBN; or CMBST	CMBST
K028	Spent catalyst from the hydrochlorinator reactor in the production of 1,1,1-trichloroethane.	1,1-Dichloroethane trans-1,2-Dichloroethylene	75–34–3 156–60–5	0.059 0.054	6.0 30
		Hexachlorobutadiene	87–68–3	0.055	5.6
		Hexachloroethane	67–72–1	0.055	30
		Pentachloroethane	76–01–7	NA	6.0
		1,1,1,2-Tetrachloroethane	630–20–6	0.057	6.0
		1,1,2,2-Tetrachloroethane	79–34–6	0.057	6.0
		Tetrachloroethylene	127–18–4	0.056	6.0
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
		1,1,2-Trichloroethane	79–00–5	0.054	6.0
		Cadmium	7440–43–9	0.69	NA
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
K029	Waste from the product steam stripper in the production of 1,1,1-trichloroethane.	Chloroform 1,2-Dichloroethane	67–66–3 107–06–2	0.046 0.21	6.0 6.0
		1,1-Dichloroethylene	75–35–4	0.025	6.0
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
		Vinyl chloride	75–01–4	0.27	6.0
K030	Column bodies or heavy ends from the combined production of trichloroethylene and perchloroethylene.	o-Dichlorobenzene p-Dichlorobenzene	95–50–1 106–46–7	0.088 0.090	NA NA
		Hexachlorobutadiene	87–68–3	0.055	5.6
		Hexachloroethane	67–72–1	0.055	30
		Hexachloropropylene	1888–71–7	NA	30
		Pentachlorobenzene	608–93–5	NA	10
		Pentachloroethane	76–01–7	NA	6.0
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	14
		Tetrachloroethylene	127–18–4	0.056	6.0
		1,2,4-Trichlorobenzene	120–82–1	0.055	19
K031	By-product salts generated in the production of MSMA and cacodylic acid.	Arsenic	7440–38–2	14	5.0 mg/L TCLP
K032	Wastewater treatment sludge from the production of chlordane.	Hexachlorocyclopentadiene Chlordane (alpha and gamma isomers)	77–47–4 57–74–9	.057 0.0033	2.4 0.26
		Heptachlor	76–44–8	0.0012	0.066
		Heptachlor epoxide	1024–57–3	0.016	0.066
K033	Wastewater and scrub water from the clorination of cyclopentadiene in the production of chlordane.	Hexachlorocyclopentadiene	77–47–4	0.057	2.4
K034	Filter solids from the filtration of hexachlorocyclopentadiene in the production of chlordane.	Hexachlorocyclopentadiene	77–47–4	0.057	2.4
K035	Wastewater treatment sludges generated in the production of cresote.	Acenaphthene Anthracene	83–32–9 120–12–7	NA NA	3.4 3.4
		Benz(a)anthracene	56–55–3	0.059	3.4
		Bemzo(a)pyrene	50–32–8	0.061	3.4
		Chrysene	218–01–9	0.059	3.4
		o-Cresol	95–48–7	0.11	5.6
		m-Cresol (difficult to distinguish from p-cresol)	108–39–4	0.77	5.6
		p-Cresol (difficult to distinguish from m-cresol)	106–44–5	0.77	5.6
		Dibenz(a,h)anthracene	53–70–3	NA	8.2
		Fluoranthene	206–44–0	0.068	3.4
		Fluorene	86–73–7	NA	3.4
		Indeno(1,2,3-cd)pyrene	193–39–5	NA	3.4
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–1	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Pyrene	129–00–0	0.067	8.2
K036	Still bottoms from toluene reclamation distillation in the production of disulfoton.	Disulfoton	298–04–4	0.017	6.2
K037	Wastewater treatment sludges from the production of disulfoton.	Disulfoton Toluene	298–04–4 108–88–3	0.017 0.080	6.2 10
K038	Wastewater from the washing and stripping of phorate production.	Phorate	298–02–2	0.021	4.6
K039	Filter cake from the filtration of diethylphorphorodithioic acid in the production of phorate.	NA	NA	CARBN; or CMBST	CMBST
K040	Wastewater treatment sludge from the production of phorate.	Phorate	298–02–2	0.021	4.6
K041	Wastewater treatment sludge from the production of toxaphene.	Toxaphene	8001–35–2	0.0095	2.6
K042	Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the production of 2,4,5-T.	o-Dichlorobenzene p-Dichlorobenzene Pentachlorobenzene	95–50–1 106–46–7 608–93–5	0.088 0.090 0.055	6.0 6.0 10
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	14
		1,2,4-Trichlorobenzene	120–82–1	0.055	19
K043	2,6-Dichlorophenol waste from the production of 2,4-D.	2,4-Dichlorophenol	120–83–2	0.044	14
		2,6-Dichlorophenol	187–65–0	0.044	14
		2,4,5-Trichlorophenol	95–95–4	0.18	7.4
		2,4,6-Trichlorophenol	88–06–2	0.035	7.4
		2,3,4,6-Tetrachlorophenol	58–90–2	0.030	7.4
		Pentachlorophenol	87–86–5	0.089	7.4
		Tetrachloroethylene	127–18–4	0.056	6.0
		HxCDDs (All Hexachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		HxCDFs (All Hexachlorodibenzofurans)	NA	0.000063	0.001
		PeCDDs (All Pentachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		PeCDFs (All Pentachlorodibenzofurans)	NA	0.000035	0.001
		TCDDs (All Tetrachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		TCDFs (All Tetrachlorodibenzofurans)	NA	0.000063	0.001
K044	Wastewater treatment sludges from the manufacturing and processing of explosives.	NA	NA	DEACT	DEACT
K045	Spent carbon from the treatment of wastewater containing explosives.	NA	NA	DEACT	DEACT
K046	Wastewater treatment sludges from the manufacturing, formulation and loading of lead-based initiating compounds.	Lead	7439–92–1	0.69	0.75 mg/L TCLP
K047	Pink/red water from TNT operations.	NA	NA	DEACT	DEACT
K048	Dissolved air flotation (DAF) float from the petroleum refining industry.	Benzene Benzo(a)pyrene	71–43–2 50–32–8	0.14 0.061	10 3.4
		bis(2-Ethylhexyl)phthalate	117–81–7	0.28	28
		Chrysene	218–01–9	0.059	3.4
		Di-n-butyl phthalate	84–74–2	0.057	28
		Ethylbenzene	100–41–4	0.057	10
		Fluorene	86–73–7	0.059	NA
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–8	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Pyrene	129–00–0	0.067	8.2
		Toluene	108–88–33	0.080	10
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Chanides (Total)⁷	57–12–5	1.2	590
		Lead	7439–92–1	0.69	NA
		Nickel	7440–02–0	NA	11 mg/L TCLP
K049	Slop oil emulsion solids from the petroleum refining industry.	Anthracene Benzene	120–12–7 71–43–2	0.059 0.14	3.4 10
		Benzo(a)pyrene	50–32–8	0.061	3.4
		bis(2-Ethylhexyl)phthalate	117–81–7	0.28	28
		Carbon disulfide	75–15–0	3.8	NA
		Chrysene	218–01–9	0.059	3.4
		2,4-Dimethylphenol	105–67–9	0.036	NA
		Ethylbenzene	100–41–4	0.057	10
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–8	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Pyrene	129–00–0	0.067	8.2
		Toluene	108–88–3	0.080	10
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Cyanides (Total)⁷	57–12–5	1.2	590
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Lead	7439–92–1	0.69	NA
		Nickel	7440–02–0	NA	11 mg/L TCLP
K050	Heat exchanger bundle cleaning sludge from the petroleum refining industry.	Benzo(a)pyrene Phenol	50–32–8 108–95–2	0.061 0.039	3.4 6.2
		Cyanides (Total)⁷	57–12–5	1.2	590
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Lead	7439–92–1	0.69	NA
		Nickel	7440–02–0	NA	11 mg/L TCLP
K051	API separator sludge from the petroleum refining industry.	Acenaphthene Anthracene	83–32–9 120–12–7	0.059 0.059	NA 3.4
		Benz(a)anthracene	56–55–3	0.059	3.4
		Benzene	71–43–2	0.14	10
		Benzo(a)pyrene	50–32–8	0.061	3.4
		bis(2-Ethylhexyl)phthalate	117–81–7	0.28	28
		Chrysene	218–01–9	0.059	3.4
		Di-n-butyl phthalate	105–67–9	0.057	28
		Ethylbenzene	100–41–4	0.057	10
		Fluorene	86–73–7	0.059	NA
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–8	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Pyrene	129–00–0	0.067	8.2
		Toluene	108–88–3	0.08	10
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Cyanides (Total)⁷	57–12–5	1.2	590
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Lead	7439–92–1	0.69	NA
		Nickel	7440–02–0	NA	11 mg/L TCLP
K052	Tank bottoms (leaded) from the petroleum refining industry.	Benzene Benzo(a)pyrene	71–43–2 50–32–8	0.14 0.061	10 3.4
		o-Cresol	95–48–7	0.11	5.6
		m-Cresol (difficult to distinguish from p-cresol)	108–39–4	0.77	5.6
		p-Cresol (difficult to distinguish from m-cresol)	106–44–5	0.77	5.6
		2,4-Dimethylphenol	105–67–9	0.036	NA
		Ethylbenzene	100–41–4	0.057	10
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–8	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Toluene	108–88–3	0.08	10
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Lead	7439–92–1	0.69	NA
		Nickel	7440–02–0	NA	11 mg/L TCLP
K060	Ammonia still lime sludge from coking operations.	Benzene	71–43–2	0.14	10
		Benzo(a)pyrene	50–32–8	0.061	3.4
		Naphthalene	91–20–3	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Cyanides (Total)⁷	57–12–5	1.2	590
K061	Emission control dust/sludge from the primary production of steel in electric furnaces.	Antimony Arsenic	7440–36–0 7440–38–2	NA NA	1.15 mg/L TCLP 5.0 mg/L TCLP
		Barium	7440–39–3	NA	21 mg/L TCLP
		Beryllium	7440–41–7	NA	1.22 mg/L TCLP
		Cadmium	7440–43–9	0.69	0.11 mg/L TCLP
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Mercury	7439–97–6	NA	0.025 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Selenium	7782–49–2	NA	5.7 mg/L TCLP
		Silver	7440–22–4	NA	0.14 mg/L TCLP
		Thallium	7440–28–0	NA	0.20 mg/L TCLP
		Zinc	7440–66–6	NA	4.3 mg/L TCLP
K062	Spent pickle liquor generated by steel finishing operations of facilities within the iron and steel industry (SIC Codes 331 and 332).	Chromium (Total) Lead Nickel	7440–47–3 7439–92–1 7440–02–0	2.77 0.69 3.98	0.60 mg/L TCLP 0.75 mg/L TCLP NA
K069	Emission control dust/sludge from secondary lead smelting—Calcium Sulfate (Low Lead) Subcategory	Cadmium Lead	7440–43–9 7439–92–1	0.69 0.69	0.11 mg/L TCLP 0.75 mg/L TCLP
	Emission control dust/sludge from secondary lead smelting—Non-Calcium Sulfate (High Lead) Subcategory	NA	NA	NA	RLEAD
K071	K071 (Brine purification muds from the mercury cell process in chlorine production, where separately prepurified brine is not used) nonwastewaters that are residues from RMERC.	Mercury	7439–97–6	NA	0.20 mg/L TCLP
	K071 (Brine purification muds from the mercury cell process in chlorine production, where separately prepurified brine is not used.) nonwastewaters that are not residues from RMERC.	Mercury	7439–97–6	NA	0.025 mg/L TCLP
	All K071 wastewaters.	Mercury	7439–97–6	0.15	NA
K073	Chlorinated hydrocarbon waste from the purification step of the diaphragm cell process using graphite anodes in chlorine production.	Carbon tetrachloride Chloroform Hexachloroethane	56–23–5 67–66–3 67–72–1	0.057 0.046 0.055	6.0 6.0 30
		Tetrachloroethylene	127–18–4	0.056	6.0
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
K083	Distillation bottoms from aniline production.	Aniline	62–53–3	0.81	14
		Benzene	71–43–2	0.14	10
		Cyclohexanone	108–94–1	0.36	NA
		Diphenylamine (difficult to distinguish from diphenylnitrosamine	122–39–4	0.92	13
		Diphenylnitrosamine (difficult to distinguish from diphenylamine)	86–30–6	0.92	13
		Nitrobenzene	98–95–3	0.068	14
		Phenol	108–95–2	0.039	6.2
		Nickel	7440–02–0	3.98	11 mg/L TCLP
K084	Wastewater treatment sludges generated during the production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.	Arsenic	7440–38–2	1.4	5.0 mg/L TCLP
K085	Distillation or fractionation column bottoms from the production of chlorobenzenes.	Benzene Chlorobenzene m-Dichlorobenzene	71–43–2 108–90–7 541–73–1	0.14 0.057 0.036	10 6.0 6.0
		o-Dichlorobenzene	95–50–1	0.088	6.0
		p-Dichlorobenzene	106–46–7	0.090	6.0
		Hexachlorobenzene	118–74–1	0.055	10
		Total PCBs (sum of all PCB isomers, or all Aroclors)	1336–36–3	0.10	10
		Pentachlorobenzene	608–93–5	0.055	10
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	14
		1,2,4-Trichlorobenzene	120–82–1	0.055	19
K086	Solvent wastes and sludges, caustic washes and sludges, or water washes and sludges from cleaning tubs and equipment used in the formulation of ink from pigments, driers, soaps, and stabilizers containing chromium and lead.	Acetone Acetophenone bis(2-Ethylhexyl) phthalate n-Butyl alcohol	67–64–1 96–86–2 117–81–7 71–36–3	0.28 0.010 0.28 5.6	160 9.7 28 2.6
		Butylbenzyl phthalate	85–68–7	0.017	28
		Cyclohexanone	108–94–1	0.36	NA
		o-Dichlorobenzene	95–50–1	0.088	6.0
		Diethyl phthalate	84–66–2	0.20	28
		Dimethyl phthalate	131–11–3	0.047	28
		Di-n-butyl phthalate	84–74–2	0.057	28
		Di-n-octyl phthalate	117–84–0	0.017	28
		Ethyl acetate	141–78–6	0.34	33
		Ethylbenzene	100–41–4	0.057	10
		Methanol	67–56–1	5.6	NA
		Methyl ethyl ketone	78–93–3	0.28	36
		Methyl isobutyl ketone	108–10–1	0.14	33
		Methylene chloride	75–09–2	0.089	30
		Naphthalene	91–20–3	0.059	5.6
		Nitrobenzene	98–95–3	0.068	14
		Toluene	108–88–3	0.080	10
		1,1,1-Trichloroethane	71–55–6	0.054	6.0
		Trichloroethylene	79–01–6	0.054	6.0
		Xylenes-mixed isomers (sum of o-, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
K087	Decanter tank tar sludge from coking operations.	Acenaphthylene	208–96–8	0.059	3.4
		Benzene	71–43–2	0.14	10
		Chrysene	218–01–9	0.059	3.4
		Fluoranthene	206–44–0	0.068	3.4
		Indeno(1,2,3-cd)pyrene	193–39–5	0.0055	3.4
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	85–01–8	0.059	5.6
		Toluene	108–88–3	0.080	10
		Xylenes-mixed isomers (sum of o, m-, and p-xylene concentrations)	1330–20–7	0.32	30
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
K088	Spent potliners from primary aluminum reduction.	Acenaphthene	83–32–9	0.059	3.4
		Anthracene	120–12–7	0.059	3.4
		Benz(a)anthracene	56–55–3	0.059	3.4
		Benzo(a)pyrene	50–32–8	0.061	3.4
		Benzo(b)fluoranthene	205–99–2	0.11	6.8
		Benzo(k)fluoranthene	207–08–9	0.11	6.8
		Benzo(g,h,i)perylene	191–24–2	0.0055	1.8
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Fluoranthene	206–44–0	0.068	3.4
		Indeno(1,2,3,-cd)pyrene	193–39–5	0.0055	3.4
		Phenanthrene	85–01–8	0.059	5.6
		Pyrene	129–00–0	0.067	8.2
		Antimony	7440–36–0	1.9	1.15 mg/L TCLP
		Arsenic	7440–38–2	1.4	26.1
		Barium	7440–39–3	1.2	21 mg/L TCLP
		Beryllium	7440–41–7	0.82	1.22 mg/L TCLP
		Cadmium	7440–43–9	0.69	0.11 mg/L TCLP
		Chromium (Total)	7440–47–3	2.77	0.60 mg/L TCLP
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Mercury	7439–97–6	0.15	0.025 mg/L TCLP
		Nickel	7440–02–0	3.98	11 mg/L TCLP
		Selenium	7782–49–2	0.82	5.7 mg/L TCLP
		Silver	7440–22–4	0.43	0.14 mg/L TCLP
		Cyanide (Total)⁷	57–12–5	1.2	590
		Cyanide (Amenable)⁷	57–12–5	0.86	30
		Fluoride	16984–48–8	35	NA
K093	Distillation light ends from the production of phthalic anhydride from ortho-xylene	Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	100–21–0	0.055	28
		Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	85–44–9	0.055	28
K094	Distillation bottoms from the production of phthalic anhydride from ortho-xylene.	Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	100–21–0	0.055	28
		Phthalic anhydride (measured as Phthalic acid or Terephthalic acid)	85–44–9	0.055	28
K095	Distillation bottoms from the production of 1,1,1-trichloroethane.	Hexachloroethane Pentachloroethane	67–72–1 76–01–7	0.055 0.055	30 6.0
		1,1,1,2-Tetrachloroethane	630–20–6	0.057	6.0
		1,1,2,2-Tetrachloroethane	79–34–6	0.057	6.0
		Tetrachloroethylene	127–18–4	0.056	6.0
		1,1,2-Trichloroethane	79–00–5	0.054	6.0
		Trichloroethylene	79–01–1	0.054	6.0
K096	Heavy ends from the heavy ends column from the production of 1,1,1-trichloroethane.	m-Dichlorobenzene Pentachloroethane	541–73–1 76–01–1	0.036 0.055	6.0 6.0
		1,1,1,2-Tetrachloroethane	630–20–6	0.057	6.0
		1,1,2,2-Tetrachloroethane	79–34–6	0.057	6.0
		Tetrachloroethylene	127–18–4	0.056	6.0
		1,2,4-Trichlorobenzene	120–82–1	0.055	19
		1,1,2-Trichloroethane	79–00–5	0.054	6.0
		Trichloroethylene	79–01–6	0.054	6.0
K097	Vacuum stripper discharge from the chlordane clorinator in the production of chlordane.	Chlordane (alpha and gamma isomers) Heptachlor	57–74–9 76–44–8	0.0033 0.0012	0.26 0.066
		Heptachlor epoxide	1024–57–3	0.016	0.066
		Hexachlorocyclopentadiene	77–47–4	0.057	2.4
K098	Untreated process wastewater from the production of toxaphene.	Toxaphene	8001–35–2	0.0095	2.6
K099	Untreated wastewater from the production of 2,4-D.	2,4-Dichlorophenoxyacetic acid	94–75–7	0.72	10
		HxCDDs (All Hexachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		HxCDFs (All Hexachlorodibenzofurans)	NA	0.000063	0.001
		PeCDDs (All Pentachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		PeCDFs (All Pentachlorodibenzofurans)	NA	0.000035	0.001
		TCDDs (All Tetrachlorodibenzo-p-dioxins)	NA	0.000063	0.001
		TCDFs (All Tetrachlorodibenzofurans)	NA	0.000063	0.001
K100	Waste leaching solution from acid leaching of emission control dust/sludge from secondary lead smelting.	Cadmium Chromium (Total) Lead	7440–43–9 7440–47–3 7439–92–1	0.69 2.77 0.69	0.11 mg/L TCLP 0.60 mg/L TCLP 0.75 mg/L TCLP
K101	Distillation tar residues from the distillation of aniline-based compounds in the production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.	o-Nitroaniline Arsenic Cadmium	88–74–4 7440–38–2 7440–43–9	0.27 1.4 0.69	14 5.0 mg/L TCLP NA
		Lead	7439–92–1	0.69	NA
		Mercury	7439–97–6	0.15	NA
K102	Residue from the use of activated carbon for decolorization in the production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.	o-Nitrophenol Arsenic Cadmium	88–75–5 7440–38–2 7440–43–9	0.028 1.4 0.69	13 5.0 mg/L TCLP NA
		Lead	7439–92–1	0.69	NA
		Mercury	7439–97–6	0.15	NA
K103	Process residues from aniline extraction from the production of aniline.	Aniline Benzene	62–53–3 71–43–2	0.81 0.14	14 10
		2,4-Dinitrophenol	51–28–5	0.12	160
		Nitrobenzene	98–95–3	0.068	14
		Phenol	108–95–2	0.039	6.2
K104	Combined wastewater streams generated from nitrobenzene/aniline production.	Aniline Benzene	62–53–3 71–43–2	0.81 0.14	14 10
		2,4-Dinitrophenol	51–28–5	0.12	160
		Nitrobenzene	98–95–3	0.068	14
		Phenol	108–95–2	0.039	6.2
		Cyanides (Total)⁷	57–12–5	1.2	590
K105	Separated aqueous stream from the reactor product washing step in the production of chlorobenzenes.	Benzene Chlorobenzene	71–43–2 108–90–7	0.14 0.057	10 6.0
		2-Chlorophenol	95–57–8	0.044	5.7
		o-Dichlorobenzene	95–50–1	0.088	6.0
		p-Dichlorobenzene	106–46–7	0.090	6.0
		Phenol	108–95–2	0.039	6.2
		2,4,5-Trichlorophenol	95–95–4	0.18	7.4
		2,4,6-Trichlorophenol	88–06–2	0.035	7.4
K106	K106 (wastewater treatment sludge from the mercury cell process in chlorine production) nonwastewaters that contain greater than or equal to 260 mg/kg total mercury.	Mercury	7439–97–6	NA	RMERC
	K106 (wastewater treatment sludge from the mercury cell process in chlorine production) nonwastewaters that contain less than 260 mg/kg total mercury that are residues from RMERC.	Mercury	7439–97–6	NA	0.20 mg/L TCLP
	Other K106 nonwastewaters that contain less than 260 mg/kg total mercury and are not residues from RMERC.	Mercury	7439–97–6	NA	0.025 mg/L TCLP
	All K106 wastewaters.	Mercury	7439–97–6	0.15	NA
K107	Column bottoms from production separation from the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.	NA	NA	CMBST; or CHOXD fb CARBN; or BIODG fb CARBN	CMBST
K108	Condensed column overheads from product separation and condensed reactor vent gases from the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.	NA	NA	CMBST; or CHOXD fb CARBN; or BIODG fb CARBN	CMBST
K109	Spent filter cartridges from product purification from the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.	NA	NA	CMBST; or CHOXD fb CARBN; or BIODG fb CARBN	CMBST
K110	Condensed column overheads from intermediate separation from the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.	NA	NA	CMBST; or CHOXD fb CARBN; or BIODG fb CARBN	CMBST
K111	Product washwaters from the production of dinitrotoluene via nitration of toluene.	2,4-Dinitrotoluene 2,6-Dinitrotoluene	121–14–2 606–20–2	0.32 0.55	140 28
K112	Reaction by-product water from the drying column in the production of toluenediamine via hydrogenation of dinitrotoluene.	NA	NA	CMBST; or CHOXD fb CARBN; or BIODG fb CARBN	CMBST
K113	Condensed liquid light ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.	NA	NA	CARBN; or CMBST	CMBST
K114	Vicinals from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.	NA	NA	CARBN; or CMBST	CMBST
K115	Heavy ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.	Nickel NA	7440–02–2 NA	3.98 CARBN; or CMBST	11 mg/L TCLP CMBST
K116	Organic condensate from the solvent recovery column in the production of toluene diisocyanate via phosgenation of toluenediamine.	NA	NA	CARBN; or CMBST	CMBST
K117	Wastewater from the reactor vent gas scrubber in the production of ethylene dibromide via bromination of ethene.	Methyl bromide (Bromomethane) Chloroform	74–83–9 67–66–3	0.11 0.046	15 6.0
		Ethylene dibromide (1,2-Dibromoethane)	106–93–4	0.028	15
K118	Spent absorbent solids from purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.	Methyl bromide (Bromomethane) Chloroform	74–83–9 67–66–3	0.11 0.046	15 6.0
		Ethylene dibromide (1,2,-Dibromoethane)	106–93–4	0.028	15
K123	Process wastewater (including supernates, filtrates, and washwaters) from the production of ethylenebisdithiocarbamic acid and its salts.	NA	NA	CMBST; or CHOXD fb (BIODG or CARBN)	CMBST
K124	Reactor vent scrubber water from the production of ethylenebisdithiocarbamic acid and its salts.	NA	NA	CMBST; or CHOXD fb (BIODG or CARBN)	CMBST
K125	Filtration, evaporation, and centrifugation solids from the production of ethylenebisdithiocarbamic acid and its salts.	NA	NA	CMBST; or CHOXD fb (BIODG or CARBN)	CMBST
K126	Baghouse dust and floor sweepings in milling and packaging operations from the production or formulation of ethylenebisdithiocarbamic acid and its salts.	NA	NA	CMBST; or CHOXD fb (BIODG or CARBN)	CMBST
K131	Wastewater from the reactor and spent sulfuric acid from the acid dryer from the production of methyl bromide.	Methyl bromide (Bromomethane)	74–83–9	0.11	15
K132	Spent absorbent and wastewater separator solids from the production of methyl bromide.	Methyl bromide (Bromomethane)	74–83–9	0.11	15
K136	Still bottoms from the purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.	Methyl bromide (Bromomethane) Chloroform	74–83–9 67–66–3	0.11 0.46	15 6.0
		Ethylene dibromide (1,2-Dibromoethane)	106–93–4	0.028	15
K141	Process residues from the recovery of coal tar, including, but not limited to, collecting sump residues from the production of coke or the recovery of coke by-products produced from coal. This listing does not include K087 (decanter tank tar sludge from coking operations).	Benzene Benz(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	71–43–2 56–55–3 50–2–8 205–99–2	0.14 0.059 0.061 0.11	10 3.4 3.4 6.8
		Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene)	207–08–9	0.11	6.8
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Indeno(1,2,3-cd)pyrene	193–39–5	0.0055	3.4
K142	Tar storage tank residues from the production of coke from coal or from the recovery of coke by-products produced from coal.	Benzene Benz(a)anthracene	71–43–2 56–55–3	0.14 0.059	10 3.4
		Benzo(a)pyrene	50–32–8	0.061	3.4
		Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	205–99–2	0.11	6.8
		Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene)	207–08–9	0.11	6.8
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Indeno(1,2,3-cd)pyrene	193–39–5	0.0055	3.4
K143	Process residues from the recovery of light oil, including, but not limited to, those generated in stills, decanters, and wash oil recovery units from the recovery of coke by-products produced from coal.	Benzene Benz(a)anthracene Benzo(a)pyrene	71–43–2 56–55–3 50–32–8	0.14 0.059 0.061	10 3.4 3.4
		Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	205–99–2	0.11	6.8
		Benzo(k)flouranthene (difficult to distinguish from benzo(b)fluoranthene	207–08–9	0.11	6.8
		Chrysene	218–01–9	0.059	3.4
K144	Wastewater sump residues from light oil refining, including, but not limited to, intercepting or contamination sump sludges from the recovery of coke by-products produced from coal.	Benzene Benz(a)pyrene Benzo(a)anthracene	71–43–2 56–55–3 50–32–8	0.14 0.059 0.061	10 3.4 3.4
		Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	205–99–2	0.11	6.8
		Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene)	207–08–9	0.11	6.8
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
K145	Residues from naphthalene collection and recovery operations from the recovery of coke by-products produced from coal.	Benzene Benz(a)anthracene	71–43–2 56–55–3	0.14 0.059	10 3.4
		Benzo(a)pyrene	50–32–8	0.061	3.4
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Naphthalene	91–20–3	0.059	5.6
K147	Tar storage tank residues from coal tar refining.	Benzene	71–43–2	0.14	10
		Benz(a)anthracene	56–55–3	0.059	3.4
		Benzo(a)pyrene	50–32–8	0.061	3.4
		Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	205–99–2	0.11	6.8
		Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene)	207–08–9	0.11	6.8
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Indeno(1,2,3-cd)pyrene	193–39–5	0.0055	3.4
K148	Residues from coal tar distillation, including, but not limited to, still bottoms.	Benz(a)anthracene Benzo(a)pyrene	56–55–3 50–32–8	0.059 0.061	3.4 3.4
		Benzo(b)fluoranthene (difficult to distinguish from benzo(k)fluoranthene)	205–99–2	0.11	6.8
		Benzo(k)fluoranthene (difficult to distinguish from benzo(b)fluoranthene)	207–08–9	0.11	6.8
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Indeno(1,2,3-cd)pyrene	193–39–5	0.0055	3.4
K149	Distillation bottoms from the production of alpha- (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups. (This waste does not include still bottoms from the distillations of benzyl chloride.)	Chlorobenzene Chloroform Chloromethane p-Dichlorobenzene Hexachlorobenzene	108–90–7 67–66–3 74–87–3 106–46–7 118–74–1	0.057 0.046 0.19 0.090 0.055	6.0 6.0 30 6.0 10
		Pentachlorobenzene	608–93–5	0.055	10
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	14
		Toluene	108–88–3	0.080	10
K150	Organic residuals, excluding spent carbon adsorbent, from the spent chlorine gas and hydrochloric acid recovery processes associated with the production of alpha- (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups.	Carbon tetrachloride Chloroform Chloromethane p-Dichlorobenzene Hexachlorobenzene	56–23–5 67–66–3 74–87–3 106–46–7 118–74–1	0.057 0.046 0.019 0.090 0.055	6.0 6.0 30 6.0 10
		Pentachlorobenzene	608–93–5	0.055	10
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	14
		1,1,2,2-Tetrachloroethane	79–34–5	0.057	6.0
		Tetrachloroethylene	127–18–4	0.056	6.0
		1,2,4-Trichlorobenzene	120–82–1	0.055	19
K151	Wastewater treatment sludges, excluding neutralization and biological sludges, generated during the treatment of wastewaters from the production of alpha- or (methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups.	Benzene Carbon tetrachloride Chloroform Hexachlorobenzene Pentachlorobenzene	71–43–2 56–23–5 67–66–3 118–74–1 608–93–5	0.14 0.057 0.046 0.055 0.055	10 6.0 6.0 10 10
		1,2,4,5-Tetrachlorobenzene	95–94–3	0.055	14
		Tetrachloroethylene	127–18–4	0.056	6.0
		Toluene	108–88–3	0.080	10
K156	Organic waste (including heavy ends, still bottoms, light ends, spent solvents, filtrates, and decantates) from the production of carbamates and carbamoyl oximes.	Acetonitrile Acetophenone Aniline	75–05–8 98–86–2 62–53–3	5.6 0.010 0.81	1.8 9.7 14
		Benomyl	17804–35–2	0.056	1.4
		Benzene	71–43–2	0.14	10
		Carbaryl	63–25–2	0.006	0.14
		Carbenzadim	10605–21–7	0.056	1.4
		Carbofuran	1563–66–2	0.006	0.14
		Carbosulfan	55285–14–8	0.028	1.4
		Chlorobenzene	108–90–7	0.057	6.0
		Chloroform	67–66–3	0.046	6.0
		o-Dichlorobenzene	95–50–1	0.088	6.0
		Methomyl	16752–77–5	0.028	0.14
		Methylene chloride	75–09–2	0.089	30
		Methyl ethyl ketone	78–93–3	0.28	36
		Naphthalene	91–20–3	0.059	5.6
		Phenol	108–95–2	0.039	6.2
		Pyridine	110–86–1	0.014	16
		Toluene	108–88–3	0.080	10
		Triethylamine	121–44–8	0.081	1.5
K157	Wastewaters (including scrubber waters, condenser waters, washwaters, and separation waters) from the production of carbamates and carbamoyl oximes.	Carbon tetrachloride Chloroform Chloromethane Methomyl	56–23–5 67–66–3 74–87–3 16752–77–5	0.057 0.046 0.19 0.028	6.0 6.0 30 0.14
		Methylene chloride	75–09–2	0.089	30
		Methyl ethyl ketone	78–93–3	0.28	36
		Pyridine	110–86–1	0.014	16
		Triethylamine	121–44–8	0.081	1.5
K158	Bag house dusts and filter/separation solids from the production of carbamates and carbamoyl oximes.	Benomyl Benzene	17804–35–2 71–43–2	0.056 0.14	1.4 10
		Carbenzadim	10605–21–7	0.056	1.4
		Carbofuran	1563–66–2	0.006	0.14
		Carbosulfan	55285–14–8	0.028	1.4
		Chloroform	67–66–3	0.046	6.0
		Methylene chloride	75–09–2	0.089	30
		Phenol	108–95–2	0.039	6.2
K159	Organics from the treatment of thiocarbamate wastes.	Benzene	71–43–2	0.14	10
		Butylate	2008–41–5	0.042	1.4
		EPTC (Eptam)	759–94–4	0.042	1.4
		Molinate	2212–67–1	0.042	1.4
		Pebulate	1114–71–2	0.042	1.4
		Vernolate	1929–77–7	0.042	1.4
K161	Purification solids (including filtration, evaporation, and centrifugation solids), baghouse dust and floor sweepings from the production of dithiocarbamate acids and their salts.	Antimony Arsenic Carbon disulfide	7440–36–0 7440–38–2 75–15–0	1.9 1.4 3.8	1.15 mg/L TCLP 5.0 mg/L TCLP 4.8 mg/L TCLP
		Dithiocarbamates (total)	NA	0.028	28
		Lead	7439–92–1	0.69	0.75 mg/L TCLP
		Nickel	7440–02–0	3.98	11.0 mg/L TCLP
		Selenium	7782–49–2	0.82	5.7 mg/L TCLP
K169	Crude oil tank sediment from petroleum refining operations.	Benz(a)anthracene	56–55–3	0.059	3.4
		Benzene	71–43–2	0.14	10
		Benzo(g,h,i)perylene	191–24–2	0.0055	1.8
		Chrysene	218–01–9	0.059	3.4
		Ethyl benzene	100–41–4	0.057	10
		Fluorene	86–73–7	0.059	3.4
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	81–05–8	0.059	5.6
		Pyrene	129–00–0	0.067	8.2
		Toluene (Methyl Benzene)	108–88–3	0.080	10
		Xylene(s) (Total)	1330–20–7	0.32	30
K170	Clarified slurry oil sediment from petroleum refining operations.	Benz(a)anthracene Benzene	56–55–3 71–43–2	0.059 0.14	3.4 10
		Benzo(g,h,i)perylene	191–24–2	0.0055	1.8
		Chrysene	218–01–9	0.059	3.4
		Dibenz(a,h)anthracene	53–70–3	0.055	8.2
		Ethyl benzene	100–41–4	0.057	10
		Fluorene	86–73–7	0.059	3.4
		Indeno(1,3,4-cd)pyrene	193–39–5	0.0055	3.4
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	81–05–8	0.059	5.6
		Pyrene	129–00–0	0.067	8.2
		Toluene (Methyl Benzene)	108–88–3	0.080	10
		Xylene(s) (Total)	1330–20–7	0.32	30
K171	Spent hydrotreating catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media).	Benz(a)anthracene Benzene Chrysene Ethyl benzene	56–55–3 71–43–2 218–01–9 100–41–4	0.059 0.14 0.059 0.057	3.4 10 3.4 10
		Naphthalene	91–20–3	0.059	5.6
		Phenanthrene	81–05–8	0.059	5.6
		Pyrene	129–00–0	0.67	8.2
		Toluene (Methyl Benzene)	108–88–3	0.080	10
		Xylene(s) (Total)	1330–20–7	0.32	30
		Arsenic	7740–38–2	1.4	5 mg/L TCLP
		Nickel	7440–02–0	3.98	11.0 mg/L TCLP
		Vanadium	7440–62–2	4.3	1.6 mg/L TCLP
		Reactive sulfides	NA	DEACT	DEACT
K172	Spent hydrorefining catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media.).	Benzene Ethyl benzene Toluene (Methyl Benzene) Xylene(s) (Total)	71–43–2 100–41–4 108–88–3 1330–20–7	0.14 0.57 0.080 0.32	10 10 10 30
		Antimony	7740–36–0	1.9	1.15 mg/L TCLP
		Arsenic	7740–38–2	1.4	5 mg/L TCLP
		Nickel	7440–02–0	3.98	11.0 mg/L TCLP
		Vanadium	7440–62–2	4.3	1.6 mg/L TCLP
		Reactive sulfides	NA	DEACT	DEACT
K174	Wastewater treatment sludges from the production of ethylene dichloride or vinyl chloride monomer.	1,2,3,4,6,7,8-Heptachlorodibenzo- p -dioxin (1,2,3,4,6,7,8-HpCDD)	35822–46–9	0.000035 or CMBST¹¹	0.0025 or CMBST¹¹
		1,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-HpCDF)	67562–39–4	0.000035 or CMBST¹¹	0.0025 or CMBST¹¹
		1,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-HpCDF)	55673–89–7	0.000035 or CMBST¹¹	0.0025 or CMBST¹¹
		HxCDDs (All Hexachlorodibenzo- p -dioxins)	34465–46–8	0.000063 or CMBST¹¹	0.001 or CMBST¹¹
		HxCDFs (All Hexachlorodibenzofurans)	55684–94–1	0.000063 or CMBST¹¹	0.001 or CMBST¹¹
		1,2,3,4,6,7,8,9-Octachlorodibenzo- p -dioxin (OCDD)	3268–87–9	0.000063 or CMBST¹¹	0.005 or CMBST¹¹
		1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)	39001–02–0	0.000063 or CMBST¹¹	0.005 or CMBST¹¹
		PeCDDs (All Pentachlorodibenzo- p -dioxins	36088–22–9	0.000063 or CMBST¹¹	0.001 or CMBST¹¹
		PeCDFs (All Pentachlorodibenzofurans)	30402–15–4	0.000035 or CMBST¹¹	0.001 or CMBST¹¹
		TCDDs (All tetachlorodibenzo- p -dioxins)	41903–57–5	0.000063 or CMBST¹¹	0.001 or CMBST¹¹
		TCDFs (All tetrachlorodibenzofurans)	55722–27–5	0.000063 or CMBST¹¹	0.001 or CMBST¹¹
		Arsenic	7440–36–0	1.4	5.0 mg/L TCLP
K175	Wastewater treatment sludge from the production of vinyl chloride monomer using mercuric chloride catalyst in an acetylene-based process	Mercury¹² pH¹²	7438–97–6	NA NA	0.025 mg/L TCLP pH≤6.0
	All K175 wastewaters	Mercury	7438–97–6	0.15	NA
K176	Baghouse filters from the production of antimony oxide, including filters from the production of intermediates (e.g., antimony metal or crude antimony oxide)	Antimony Arsenic Cadmium Lead Mercury	7440–36–0 7440–38–2 7440–43–9 7439–92–1 7439–97–6	1.9 1.4 0.69 0.69 0.15	1.15 mg/L TCLP 5.0 mg/L TCLP 0.11 mg/L TCLP 0.75 mg/L TCLP 0.025 mg/L TCLP
K177	Slag from the production of antimony oxide that is speculatively accumulated or disposed, including slag from the production of intermediates (e.g., antimony metal or crude antimony oxide)	Antimony Arsenic Lead	7440–36–0 7440–38–2 7439–92–1	1.9 1.4 0.69	1.15 mg/L TCLP 5.0 mg/L TCLP 0.75 mg/L TCLP
K178	Residues from manufacturing and manufacturing-site storage of ferric chloride from acids formed during the production of titanium dioxide using the chloride-ilmenite process.	1,2,3,4,6,7,8- Heptachlorodibenzo- p -dioxin (1,2,3,4,6,7,8-HpCDD) 1,2,3,4,6,7,8- Heptachlorodibenzofuran (1,2,3,4,6,7,8-HpCDF) 1,2,3,4,7,8,9- Heptachlorodibenzofuran (1,2,3,4,7,8,9-HpCDF)	35822–39–4 67562–39–4 55673–89–7	0.000035 or CMBST¹¹ 0.000035 or CMBST¹¹ 0.000035 or CMBST¹¹	0.0025 or CMBST¹¹ 0.0025 or CMBST¹¹ 0.0025 or CMBST¹¹
		HxCDDs (All Hexachlorodibenzo- p -dioxins)	34465–46–8	0.000063 or CMBST¹¹	0.001 or CMBST¹¹

		HxCDFs (All Hexachlorodibenzo-furans)	55684–94–1	0.000063 or CMBST¹¹	0.001 or CMBST¹¹

		1,2,3,4,6,7,8,9- Octachlorodibenzo- p -dioxin (OCDD)	3268–87–9	0.000063 or CMBST¹¹	0.005 or CMBST¹¹

		1,2,3,4,6,7,8,9- Octachlorodibenzofuran (OCDF)	39001–02–0	0.000063 or CMBST¹¹	0.005 or CMBST¹¹

		PeCDDs (All Pentachlorodibenzo- p -dioxins)	36088–22–9	0.000063 or CMBST¹¹	0.001 or CMBST¹¹

		PeCDFs (All Pentachlorodibenzo-furans)	30402–15–4	0.000035 or CMBST¹¹	0.001 or CMBST¹¹

		TCDDs (All tetrachlorodibenzo- p -dioxins)	41903–57–5	0.000063 or CMBST¹¹	0.001 or CMBST¹¹

		TCDFs (All tetrachlorodibenzo-furans)	55722–27–5	0.000063 or CMBST¹¹	0.001 or CMBST¹¹

		Thallium	7440–28–0	1.4	0.20 mg/L TCLP

K181	Nonwastewaters from the production of dyes and/or pigments (including nonwastewaters commingled at the point of generation with nonwastewaters from other processes) that, at the point of generation, contain mass loadings of any of the constituents identified in paragraph (c) of section 261.32 that are equal to or greater than the corresponding paragraph (c) levels, as determined on a calendar year basis	Aniline o-Anisidine (2-methoxyaniline) 4-Chloroaniline p-Cresidine 2,4-Dimethylaniline (2,4-xylidine) 1,2-Phenylenediamine	62–53–3 90–04–0 106–47–8 120–71–8 95–68–1 95–54–5	0.81 0.010 0.46 0.010 0.010 CMBST; or CHOXD fb (BIODG or CARBN); or BIODG fb CARBN	14 0.66 16 0.66 0.66 CMBST; or CHOXD fb (BIODG or CARBN); or BIODG fb CARBN
		1,3-Phenylenediamine	108–45–2	0.010	0.66
P001	Warfarin, & salts, when present at concentrations greater than 0.3%	Warfarin	81–81–2	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P002	1-Acetyl-2-thiourea	1-Acetyl-2-thiourea	591–08–2	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P003	Acrolein	Acrolein	107–02–8	0.29	CMBST
P004	Aldrin	Aldrin	309–00–2	0.021	0.066
P005	Allyl alcohol	Allyl alcohol	107–18–6	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P006	Aluminum phosphide	Aluminum phosphide	20859–73–8	CHOXD; CHRED; or CMBST	CHOXD; CHRED; or CMBST
P007	5-Aminomethyl 3-isoxazolol	5-Aminomethyl 3-isoxazolol	2763–96–4	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P008	4-Aminopyridine	4-Aminopyridine	504–24–5	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P009	Ammonium picrate	Ammonium picrate	131–74–8	CHOXD; CHRED; CARBN; BIODG; or CMBST	CHOXD; CHRED; or CMBST
P010	Arsenic acid	Arsenic	7440–38–2	1.4	5.0 mg/L TCLP
P011	Arsenic pentoxide	Arsenic	7440–38–2	1.4	5.0 mg/L TCLP
P012	Arsenic trioxide	Arsenic	7440–38–2	1.4	5.0 mg/L TCLP
P013	Barium cyanide	Barium	7440–39–3	NA	21 mg/L TCLP
		Cyanides (Total)⁷	57–12–5	1.2	590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
P014	Thiophenol (Benzene thiol)	Thiophenol (Benzene thiol)	108–98–5	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P015	Beryllium dust	Beryllium	7440–41–7	RMETL; or RTHRM	RMETL; or RTHRM
P016	Dichloromethyl ether (Bis(chloromethyl)ether)	Dichloromethyl ether	542–88–1	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P017	Bromoacetone	Bromoacetone	598–31–2	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P018	Brucine	Brucine	357–57–3	(WETOX or CHOXD) fb CARBN; or CMBST	CMBST
P020	2-sec-Butyl-4,6-dinitrophenol (Dinoseb)	2-sec-Butyl-4,6-dinitrophenol (Dinoseb)	88–85–7	0.066	2.5
P021	Calcium cyanide	Cyanides (Total)⁷	57–12–5	1.2	590
		Cyanides (Amenable)⁷	57–12–5	0.86	30
P022	Carbon disulfide	Carbon disulfide	75–15–0	3.8	CMBST
&nbs

PART 268—LAND DISPOSAL RESTRICTIONS

Subpart A—General

§ 268.1 Purpose, scope, and applicability.

§ 268.2 Definitions applicable in this part.

§ 268.3 Dilution prohibited as a substitute for treatment.

§ 268.4 Treatment surface impoundment exemption.

§ 268.5 Procedures for case-by-case extensions to an effective date.

§ 268.6 Petitions to allow land disposal of a waste prohibited under subpart C of part 268.

§ 268.7 Testing, tracking, and recordkeeping requirements for generators, treaters, and disposal facilities.

§ 268.8 [Reserved]

§ 268.9 Special rules regarding wastes that exhibit a characteristic.

Subpart B—Schedule for Land Disposal Prohibition and Establishment of Treatment Standards

§§ 268.10-268.12 [Reserved]

§ 268.13 Schedule for wastes identified or listed after November 8, 1984.

§ 268.14 Surface impoundment exemptions.

Subpart C—Prohibitions on Land Disposal

§ 268.20 Waste specific prohibitions—Dyes and/or pigments production wastes.

§§ 268.21-268.29 [Reserved]

§ 268.30 Waste specific prohibitions—wood preserving wastes.

§ 268.31 Waste specific prohibitions—Dioxin-containing wastes.

§ 268.32 Waste specific prohibitions—Soils exhibiting the toxicity characteristic for metals and containing PCBs.

§ 268.33 Waste specific prohibitions—chlorinated aliphatic wastes.

§ 268.34 Waste specific prohibitions—toxicity characteristic metal wastes.

§ 268.35 Waste specific prohibitions—petroleum refining wastes.

§ 268.36 Waste specific prohibitions—inorganic chemical wastes

§ 268.37 Waste specific prohibitions—ignitable and corrosive characteristic wastes whose treatment standards were vacated.

§ 268.38 Waste specific prohibitions—newly identified organic toxicity characteristic wastes and newly listed coke by-product and chlorotoluene production wastes.

§ 268.39 Waste specific prohibitions—spent aluminum potliners; reactive; and carbamate wastes.

Subpart D—Treatment Standards

§ 268.40 Applicability of treatment standards.